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4,4',5,5'-四苯基-3,3'-[亚甲基双(硫烷二基)]双-(4H-1,2,4-三唑)

4,4',5,5'-Tetra-phenyl-3,3'-[methyl-idene-bis(sulfanedi-yl)]bis-(4H-1,2,4-triazole).

作者信息

Zhao Bing, Liu Zhuo, Gao Yan, Song Bo, Deng Qi-Gang

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Oct 20;66(Pt 11):o2814. doi: 10.1107/S1600536810040729.

DOI:10.1107/S1600536810040729
PMID:21589005
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3009284/
Abstract

The asymmetric unit of the title compound, C(29)H(22)N(6)S(2), contains one half-mol-ecule situated on a twofold rotational axis. The two triazole rings form a dihedral angle of 27.6 (2)°. In the crystal, weak inter-molecular C-H⋯N hydrogen bonds link the mol-ecules into ribbons extending along [001].

摘要

标题化合物C(29)H(22)N(6)S(2)的不对称单元包含位于二重旋转轴上的半个分子。两个三唑环形成的二面角为27.6 (2)°。在晶体中，弱的分子间C—H⋯N氢键将分子连接成沿[001]方向延伸的带状结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/23d7/3009284/ce27e31d6a76/e-66-o2814-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/23d7/3009284/ce27e31d6a76/e-66-o2814-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/23d7/3009284/ce27e31d6a76/e-66-o2814-fig1.jpg

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A short history of SHELX.SHELX简史。
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