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3 - [(4 - 苯氧基 - 苯基)硫烷基] - 5 - 苯基 - 1H - 1,2,4 - 三唑

3-[(4-Phen-oxy-phen-yl)sulfan-yl]-5-phenyl-1H-1,2,4-triazole.

作者信息

Ben Othman Raja, Marchivie Mathieu, Suzenet Franck, Routier Sylvain

机构信息

École Supérieure des Sciences et de Technologie de Hammam Sousse (ESST), Rue Lamine Abassi 4011 Hammam Sousse, Laboratoire d'Application de la Chimie aux Ressources et Substances Naturelles et l'Environnement (LACReSNE), Faculté des Sciences de Bizerte, 7021 Zarzouna, Bizerte, Tunisia ; Institut de Chimie Organique et Analytique, Université d'Orléans, UMR CNRS 7311, BP 6759, 45067 Orléans Cedex 2, France.

ICMCB CNRS UPR 9048, Université de Bordeaux, 87 Avenue du Docteur Schweitzer, 33608 Pessac Cedex, France.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2014 Apr 30;70(Pt 5):o622-3. doi: 10.1107/S1600536814008204. eCollection 2014 May 1.

DOI:10.1107/S1600536814008204
PMID:24860412
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4011301/
Abstract

The title compound, C20H15N3OS, is V-shaped. In the 4-phen-oxy-phenyl group, the two rings are inclined to one another by 74.52 (13)°. These rings are inclined to the triazole ring by 72.20 (15) and 72.30 (15)°, respectively. The phenyl ring is inclined to the triazole ring by 10.85 (12)°. In the crystal, mol-ecules are linked via N-H⋯N hydrogen bonds, forming chains propagating along [010]. These chains are linked via pairs of C-H⋯S hydrogen bonds, forming sheets lying parallel to the ac plane.

摘要

标题化合物C₂₀H₁₅N₃OS呈V形。在4-苯氧基苯基中，两个环彼此倾斜74.52 (13)°。这些环分别与三唑环倾斜72.20 (15)°和72.30 (15)°。苯环与三唑环倾斜10.85 (12)°。在晶体中，分子通过N-H⋯N氢键相连，形成沿[010]方向延伸的链。这些链通过成对的C-H⋯S氢键相连，形成平行于ac平面的片层。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/5f4959dab780/e-70-0o622-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/a267300c559d/e-70-0o622-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/f27eea444d52/e-70-0o622-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/5f4959dab780/e-70-0o622-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/a267300c559d/e-70-0o622-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/f27eea444d52/e-70-0o622-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb4f/4011301/5f4959dab780/e-70-0o622-fig3.jpg

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