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catena-Poly[[(benzoato-κO,O')(2,2'-bipyridine-κN,N')lead(II)]-μ(3)-nitrato-κO:O,O':O''].

作者信息

Yang Juan, Dai Jun, Wang Xiaohan

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Nov 27;66(Pt 12):m1686. doi: 10.1107/S160053681004907X.

DOI:10.1107/S160053681004907X
PMID:21589342
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3011738/
Abstract

In the title coordination polymer, Pb(C(7)H(5)O(2))(NO(3))(C(10)H(8)N(2)), the Pb(II) ion is eight-coordinated by two N atoms from one 2,2'-bipyridine ligand, two O atoms from one benzoate anion and four O atoms from three nitrate groups (one chelating, two bridging) in a distorted dodecahedral geometry. Adjacent Pb(II) ions are linked by bridging nitrate O atoms through the central Pb(2)O(2) and Pb(2)O(4)N(2) cores, resulting in an infinite chain structure along the b axis. The crystal structure is stabilized by π-π stacking inter-actions between 2,2'-bipyridine and benzoate ligands belonging to neighboring chains, with shortest centroid-centroid distances of 3.685 (8) and 3.564 (8) Å.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8157/3011738/ee1e31cfbef6/e-66-m1686-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8157/3011738/730ea6022385/e-66-m1686-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8157/3011738/ee1e31cfbef6/e-66-m1686-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8157/3011738/730ea6022385/e-66-m1686-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8157/3011738/ee1e31cfbef6/e-66-m1686-fig2.jpg

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