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（R(p)）-2-异丙基-5-甲基-环己基异丙基（苯基）次膦酸酯

(R(p))-2-Isopropyl-5-methyl-cyclo-hexyl isoprop-yl(phen-yl)phosphinate.

作者信息

Liu Li-Juan, Xu Hao, Meng Fan-Jie, Wang Da-Qi, Zhao Chang-Qiu

机构信息

College of Chemistry and Chemical Engineering, Liaocheng University, Shandong 252059, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 May 1;67(Pt 5):o1186. doi: 10.1107/S1600536811013390. Epub 2011 Apr 22.

DOI:10.1107/S1600536811013390
PMID:21754488
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3089224/
Abstract

The title compound, C(19)H(31)O(2)P, features a distorted tetra-hedral P atom that bonds to the phenyl ring, isopropyl and 2-isopropyl-5-methyl-cyclo-hexyl groups, and is determined as having an R(p) configuration. A chair conformation is observed for the cyclo-hexyl ring. In the crystal, mol-ecules are linked into chains running along the a axis by weak inter-molecular C-H⋯O hodrogen bonds.

摘要

标题化合物C(19)H(31)O(2)P的特征是一个扭曲的四面体磷原子，它与苯环、异丙基和2-异丙基-5-甲基环己基相连，并确定具有R(p)构型。观察到环己基环呈椅式构象。在晶体中，分子通过弱分子间C-H⋯O氢键连接成沿a轴延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dc36/3089224/8410eacdbc8f/e-67-o1186-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dc36/3089224/9f07430372c6/e-67-o1186-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dc36/3089224/8410eacdbc8f/e-67-o1186-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dc36/3089224/9f07430372c6/e-67-o1186-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dc36/3089224/8410eacdbc8f/e-67-o1186-fig2.jpg

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本文引用的文献

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2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.