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9-{[4-(二甲基氨基)-苄基]氨基}-5-(3,4,5-三甲氧基苯基)-5,5a,8a,9-四氢呋喃并[3',4':6,7]萘并[2,3-d][1,3]二氧杂环戊烯-6(8H)-酮

9-{[4-(Dimethyl-amino)-benz-yl]amino}-5-(3,4,5-trimeth-oxy-phen-yl)-5,5a,8a,9-tetra-hydro-furo[3',4':6,7]naphtho-[2,3-d][1,3]dioxol-6(8H)-one.

作者信息

Li Yan, Wang Huo, Chen Hong, Chen Li-Ting, Liu Jing

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1538-9. doi: 10.1107/S1600536811019234. Epub 2011 May 28.

DOI:10.1107/S1600536811019234
PMID:21754898
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3120627/
Abstract

In the title compound, C(31)H(34)N(2)O(7), the fused tetra-hydro-furan and six-membered rings each display an envelope conformation. The dihedral angles between the benzene ring of the benzo[d][1,3]dioxole and the other two benzene rings are 89.68 (3) and 63.38 (2)°. In the crystal, weak inter-molecular C-H⋯O hydrogen bonds link the mol-ecules.

摘要

在标题化合物C(31)H(34)N(2)O(7)中，稠合的四氢呋喃环和六元环均呈信封式构象。苯并[d][1,3]二氧戊环的苯环与另外两个苯环之间的二面角分别为89.68 (3)°和63.38 (2)°。在晶体中，分子间通过弱C—H⋯O氢键相连。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a144/3120627/b9894d0cf627/e-67-o1538-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a144/3120627/b9894d0cf627/e-67-o1538-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a144/3120627/b9894d0cf627/e-67-o1538-fig1.jpg

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