CEMES-CNRS and Université de Toulouse, 29 rue Jeanne Marvig, F-31055 Toulouse, France.
Ultramicroscopy. 2011 Jul;111(8):1328-37. doi: 10.1016/j.ultramic.2011.04.008. Epub 2011 Apr 30.
The genesis, theoretical basis and practical application of the new electron holographic dark-field technique for mapping strain in nanostructures are presented. The development places geometric phase within a unified theoretical framework for phase measurements by electron holography. The total phase of the transmitted and diffracted beams is described as a sum of four contributions: crystalline, electrostatic, magnetic and geometric. Each contribution is outlined briefly and leads to the proposal to measure geometric phase by dark-field electron holography (DFEH). The experimental conditions, phase reconstruction and analysis are detailed for off-axis electron holography using examples from the field of semiconductors. A method for correcting for thickness variations will be proposed and demonstrated using the phase from the corresponding bright-field electron hologram.
本文介绍了用于纳米结构应变映射的新型电子全息暗场技术的起源、理论基础和实际应用。该发展将几何相位置于电子全息相位测量的统一理论框架内。透射和衍射光束的总相位可以表示为四个分量的和:晶体、静电、磁场和几何相位。简要概述了每个分量,并提出通过暗场电子全息术(DFEH)测量几何相位。详细介绍了使用半导体领域的示例进行离轴电子全息术的实验条件、相位重构和分析。将提出并演示一种用于校正厚度变化的方法,该方法使用相应的明场电子全息图的相位。