Yang Jian, Ma Yanni, Pan Meng, Cao Fangjun, Zhou Le
College of Science, Northwest Agriculture and Forest University, Yangling 712100, People's Republic of China.
Acta Crystallogr Sect E Struct Rep Online. 2011 Oct 1;67(Pt 10):o2721. doi: 10.1107/S160053681103710X. Epub 2011 Sep 30.
There are two independent mol-ecules in the asymmetric unit of the title compound, C(15)H(13)NO(2), in both the six-membered dihydro-pyridine rings adopt a half-chair conformation. The two benzene rings make dihedral angles of 43.66 (10) and 62.22 (10)° in the two mol-ecules. In the crystal, the two independent mol-ecules are linked alternately by inter-molecular O-H⋯O hydrogen bonds, forming a zigzag chain along the c axis. Furthermore, inter-molecular C-H⋯π inter-actions link the chains into a three-dimensional network.
标题化合物C(15)H(13)NO(2)的不对称单元中有两个独立分子,六元二氢吡啶环均呈半椅式构象。两个苯环在两个分子中的二面角分别为43.66 (10)°和62.22 (10)°。在晶体中,两个独立分子通过分子间O-H⋯O氢键交替连接,沿c轴形成之字形链。此外,分子间C-H⋯π相互作用将这些链连接成三维网络。