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2-氰基-N'-(2-羟基-3-甲氧基亚苄基)乙酰肼

2-Cyano-N'-(2-hy-droxy-3-meth-oxy-benzyl-idene)acetohydrazide.

作者信息

Li Hongbo, Chen Peng

机构信息

College of Chemistry and Biology Engineering, Yancheng Institute of Technology, Yancheng 224051, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Aug 1;67(Pt 8):o2001. doi: 10.1107/S1600536811025451. Epub 2011 Jul 9.

DOI:10.1107/S1600536811025451
PMID:22091035
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3213456/
Abstract

The title compound, C(11)H(11)N(3)O(3), was obtained by the reaction of 3-meth-oxy-salicyl-aldehyde with cyano-acetohydrazide in methanol. There is an intra-molecular O-H⋯N hydrogen bond in the mol-ecule. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds, generating chains running along the b axis.

摘要

标题化合物C(11)H(11)N(3)O(3)是通过3-甲氧基水杨醛与氰基乙酰肼在甲醇中反应得到的。分子内存在O-H⋯N氢键。在晶体中，分子通过N-H⋯O氢键相连，形成沿b轴延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7997/3213456/106f69d6c86d/e-67-o2001-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7997/3213456/916dd9d655d5/e-67-o2001-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7997/3213456/106f69d6c86d/e-67-o2001-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7997/3213456/916dd9d655d5/e-67-o2001-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7997/3213456/106f69d6c86d/e-67-o2001-fig2.jpg

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