含硅烷和硫代磷酸单体的引物对增强型陶瓷粘结树脂的影响。

Effects of primer containing silane and thiophosphate monomers on bonding resin to a leucite-reinforced ceramic.

机构信息

Department of Applied Prosthodontics, Graduate School of Biomedical Sciences, Nagasaki University, Nagasaki, Japan.

出版信息

J Dent. 2012 May;40(5):353-8. doi: 10.1016/j.jdent.2011.12.003. Epub 2011 Dec 9.

DOI:10.1016/j.jdent.2011.12.003

PMID:22178629

Abstract

OBJECTIVES

Silane primers are commonly used for bonding between resin-based luting agents and ceramic restorations. The purpose of the present study was to evaluate the effects of nine silane primers on the bond strength of resin to a leucite-reinforced ceramic.

METHODS

The commercially available dental primers used were five silane primers (GC Ceramic Primer, GP; Clearfil Ceramic Primer, CP; Tokuso Ceramic Primer, TP; Porcelain Liner M, PM; and Monobond Plus, MB). Four experimental primers (MDS, MTS, MDS/MPII, and MTS/MPII) and two control primers (MMA and MMA/MPII) were also prepared. The ceramic specimen was ground with silicon carbide paper, primed, and then bonded to a resin composite disc using a dual-curing luting agent. After a 24-h immersion in water, the shear bond strengths were determined.

RESULTS

Shear bond testing revealed that the bond strength was significantly improved with the use of a MTS/MPII primer when compared to MDS, MTS, MMA, MDS/MPII and MMA/MPII. Although no significant differences were detected between GP, CP, PM, and MB, the primers CP, TP, PM, and MTS/MPII exhibited the highest bond strengths, followed by GP and MB, whilst the no-primer control resulted in the lowest values.

CONCLUSION

The maximum bond strengths were obtained with CP, TP, PM, and MTS/MPII. It was suggested that the thiophosphate monomer accelerated the role of the silane monomer. When selecting a primer to bond ceramic restorations, clinicians should be aware that not only the silane monomer but also additional components of the primer considerably affect the bond strength.

摘要

目的

硅烷偶联剂通常用于树脂基水门汀和陶瓷修复体之间的粘结。本研究的目的是评估 9 种硅烷偶联剂对树脂与锂辉石增强陶瓷粘结强度的影响。

方法

使用的市售牙科偶联剂有 5 种硅烷偶联剂（GC 陶瓷偶联剂、GP；Clearfil Ceramic Primer，CP；Tokuso Ceramic Primer，TP；Porcelain Liner M，PM；和 Monobond Plus，MB）。还制备了 4 种实验偶联剂（MDS、MTS、MDS/MPII 和 MTS/MPII）和 2 种对照偶联剂（MMA 和 MMA/MPII）。陶瓷试件用碳化硅砂纸打磨，涂偶联剂，然后用双固化水门汀粘结到树脂复合盘上。水浸泡 24 小时后，测定剪切粘结强度。

结果

剪切粘结试验表明，与 MDS、MTS、MMA、MDS/MPII 和 MMA/MPII 相比，使用 MTS/MPII 偶联剂可显著提高粘结强度。虽然 GP、CP、PM 和 MB 之间没有显著差异，但 CP、TP、PM 和 MTS/MPII 表现出的粘结强度最高，其次是 GP 和 MB，而无偶联剂对照的粘结强度最低。