N-(2-Chloro-4-nitro-phen-yl)maleamic acid monohydrate.
作者信息
Shakuntala K, Fronc Marek, Gowda B Thimme, Kožíšek Jozef
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2012 Jan;68(Pt 1):o99-o100. doi: 10.1107/S1600536811052573. Epub 2011 Dec 14.
Abstract
The title compound, C(10)H(7)ClN(2)O(5)·H(2)O, crystallizes with a half-mol-ecule each of N-(2-chloro-4-nitro-phen-yl)maleamic acid (located on a mirror plane) and water (located on a twofold rotation axis) in the asymmetric unit. The main mol-ecule is planar by symmetry and its conformation is stabilized by an intra-molecular O-H⋯O hydrogen bond. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds link the mol-ecules into a three-dimensional network.
摘要
相似文献
1
N-(2-Chloro-4-nitro-phen-yl)maleamic acid monohydrate.
Acta Crystallogr Sect E Struct Rep Online. 2012 Jan;68(Pt 1):o99-o100. doi: 10.1107/S1600536811052573. Epub 2011 Dec 14.
2
N-(3-Nitro-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 16;66(Pt 7):o1671-2. doi: 10.1107/S1600536810022245.
3
N-(2,4,5-Trichloro-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 16;66(Pt 1):o182-3. doi: 10.1107/S1600536809052520.
4
N-(3-Chloro-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 16;66(Pt 7):o1643. doi: 10.1107/S1600536810021446.
5
N-(4-Chloro-3-nitro-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o873. doi: 10.1107/S1600536812008021. Epub 2012 Feb 29.
6
N-(4-Meth-oxy-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 5;66(Pt 7):o1529-30. doi: 10.1107/S1600536810019999.
7
(E)-1-[1-(3-Chloro-phen-yl)ethyl-idene]-2-(2,4-dinitro-phen-yl)hydrazine.
Acta Crystallogr Sect E Struct Rep Online. 2012 Mar 1;68(Pt 3):o704-5. doi: 10.1107/S160053681200548X. Epub 2012 Feb 17.
8
Crystal structures of three N-(aryl-sulfon-yl)-4-fluoro-benzamides.
Acta Crystallogr E Crystallogr Commun. 2016 Mar 31;72(Pt 4):575-82. doi: 10.1107/S2056989016005089. eCollection 2016 Apr 1.
9
Ethyl 5-amino-1-(4-chloro-2-nitro-phen-yl)-1H-pyrazole-4-carboxyl-ate.
Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 10;65(Pt 2):o275-6. doi: 10.1107/S1600536809000488.
10
Ethyl 2-[4-(morpholin-4-yl)phen-yl]-1-[3-(2-oxopyrrolidin-1-yl)prop-yl]-1H-1,3-benzimidazole-5-carboxyl-ate monohydrate.
Acta Crystallogr Sect E Struct Rep Online. 2012 Oct 1;68(Pt 10):o2967-8. doi: 10.1107/S1600536812039268. Epub 2012 Sep 22.
本文引用的文献
1
N-(4-Chloro-2-methyl-phen-yl)maleamic acid.
Acta Crystallogr Sect E Struct Rep Online. 2011 Dec 1;67(Pt 12):o3317. doi: 10.1107/S1600536811047817. Epub 2011 Nov 16.
2
Structure validation in chemical crystallography.
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
3
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
Zotero 插件