Xu D M, He C H, Wang S Q, Huang E X, Xu M L, Wen X G
Institute of Traditional Chinese Medicine and Materia Medica of Jilin Province, Chang Chun.
Yao Xue Xue Bao. 1990;25(2):127-30.
A new C-nor-D-homosteroid alkaloid, C27H43O6N, mp 171.5-173 degrees C, named pingbeimine C, was isolated from the bulb of Fritillaria ussuriensis Maxim. On the basis of IR, MS, 1HNMR and 13CNMR spectroscopic data, particularly X-ray crystallographic analysis, structure IV has been assigned to this alkaloid.
从乌苏里贝母的鳞茎中分离出一种新的C-去甲-D-高甾族生物碱,化学式为C27H43O6N,熔点171.5 - 173℃,命名为平贝碱C。基于红外光谱、质谱、1H核磁共振和13C核磁共振光谱数据,特别是X射线晶体学分析,已确定该生物碱的结构为IV。