Department of Food Science & Technology, Kyungpook National University, Daegu 702-701, Republic of Korea.
J Food Sci. 2012 Apr;77(4):C476-80. doi: 10.1111/j.1750-3841.2011.02614.x. Epub 2012 Mar 6.
Thermoluminescence (TL) analysis was applied to identify gamma-irradiated garlic powder in Korean barbeque sauce before and after pasteurization (85 °C, 30 min), when blended in different ratios (1%, 3%, and 5%). The sauce sample with nonirradiated garlic powder gave a background glow curve. However, the sample blended with irradiated ingredient (1 and 10 kGy) showed typical TL glow curves at temperatures of 150 to 200 °C. The identification properties of sauce samples were more influenced by blending ratios than by irradiation doses, showing that 3% and 5% added samples produced glow curves at 150 to 250 °C. After pasteurization of the samples containing the irradiated ingredient, TL glow intensity decreased but did not change its shape or temperature range. As a result, the pasteurization of Barbeque sauces containing irradiated ingredients had reduced TL glow intensity, but the shape and temperature range of glow curve were still able to provide information required for confirming irradiation treatment.
To monitor the irradiated food in international market, thermoluminescence (TL) analysis is considered most promising identification technique because of its sensitivity and long-term stability. In this study the applicability of TL analysis to detect an irradiated ingredient (garlic powder) added in low quantity to a food matrix (sauce) was investigated. The effect of processing (pasteurization) on TL results was also evaluated.
本研究采用热释光(TL)分析方法,对巴氏杀菌(85°C,30 分钟)前后、不同混合比例(1%、3%和 5%)的韩国烤肉酱中辐照大蒜粉进行鉴定。未辐照大蒜粉的酱样品产生背景发光曲线。然而,与辐照成分(1 和 10 kGy)混合的样品在 150 至 200°C 的温度下显示出典型的 TL 发光曲线。与辐照剂量相比,酱样品的识别特性受混合比例的影响更大,表明添加 3%和 5%的样品在 150 至 250°C 之间产生发光曲线。在含有辐照成分的样品经过巴氏杀菌后,TL 发光强度降低,但形状和发光曲线的温度范围没有改变。因此,辐照成分的烤肉酱经过巴氏杀菌后,TL 发光强度降低,但发光曲线的形状和温度范围仍能提供确认辐照处理所需的信息。
为了在国际市场上监测辐照食品,热释光(TL)分析被认为是最有前途的鉴定技术,因为它具有灵敏度和长期稳定性。本研究探讨了 TL 分析在检测添加到食品基质(酱汁)中的低剂量辐照成分(大蒜粉)中的应用。还评估了加工(巴氏杀菌)对 TL 结果的影响。