Jo Deokjo, Kim Byeong-Keun, Kausar Tusneem, Kwon Joong-Ho
Department of Food Science and Technology, Kyungpook National University, Daegu, Korea.
J Agric Food Chem. 2008 Feb 27;56(4):1180-3. doi: 10.1021/jf072568y. Epub 2008 Feb 2.
Photostimulated luminescence (PSL) and thermo-luminescence (TL) analyses were conducted to detect irradiated kiwifruits. Samples were irradiated with Co-60 gamma-rays at 0-2 kGy. The freeze-dried kiwifruit peel showed 309 photon counts (PCs) for nonirradiated samples that accounted for less than the lower threshold value (700 counts/60 s, negative) and above 9306 PCs for 1 and 2 kGy-irradiated samples, which was higher than the upper threshold value (5000 counts/60 s, positive). However, PSL signals of irradiated samples remarkably decreased after 6 weeks of storage. The TL measurement using minerals isolated from the whole kiwifruit surface revealed a glow curve (TL 1) with a low intensity at 200-300 degrees C in nonirradiated samples but with a higher intensity at around 180 degrees C in irradiated samples at 1 kGy or more. The TL ratios, integrated areas of TL 1/TL 2 that was measured after 1 kGy re-irradiation for the TL 1-tested minerals, were less than 0.1 in nonirradiated samples and higher than 0.1 in irradiated ones and could verify TL 1 results. The inorganic dust minerals used were mainly composed of feldspar and quartz.
进行了光激发发光(PSL)和热释光(TL)分析以检测辐照过的猕猴桃。样品用钴 - 60γ射线在0 - 2千戈瑞剂量下进行辐照。冻干的猕猴桃果皮,未辐照样品显示309个光子计数(PCs),低于下限阈值(700计数/60秒,阴性),而1千戈瑞和2千戈瑞辐照的样品PCs高于9306,高于上限阈值(5000计数/60秒,阳性)。然而,辐照样品的PSL信号在储存6周后显著下降。使用从整个猕猴桃表面分离出的矿物质进行的TL测量显示,未辐照样品在200 - 300摄氏度有一条低强度的发光曲线(TL 1),而1千戈瑞及以上辐照样品在180摄氏度左右有更高强度的发光曲线。对于经TL 1测试的矿物质,在1千戈瑞再辐照后测量的TL 1/TL 2的积分面积,即TL比率,未辐照样品小于0.1,辐照样品大于0.1,并且可以验证TL 1的结果。所使用的无机粉尘矿物质主要由长石和石英组成。