School of Physics, The University of Melbourne, Victoria 3010, Australia.
Phys Rev Lett. 2012 Feb 17;108(7):073901. doi: 10.1103/PhysRevLett.108.073901. Epub 2012 Feb 14.
Ptychographic coherent diffractive imaging (CDI) has been extensively applied using both x rays and electrons. The extension to atomic resolution has been elusive. This Letter demonstrates ptychographic electron diffractive imaging at atomic resolution, permitting identification of structure in a boron nitride helical cone at a resolution of order 1 Å, beyond that of comparative Z-contrast images. A scanning transmission electron microscope is used to create a diverging illumination in a defocused Fresnel CDI geometry, providing a robust strategy leading to a unique solution.
相衬衍射成像(CDI)已经被广泛应用于 X 射线和电子。但将其扩展到原子分辨率一直难以实现。本文展示了原子分辨率的相衬电子衍射成像,能够以 1Å 量级的分辨率识别氮化硼螺旋锥的结构,超过了比较的 Z 对比度图像。通过在离焦菲涅耳 CDI 几何中的扫描透射电子显微镜产生发散照明,提供了一种稳健的策略,从而得到了独特的解决方案。