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选择性激光熔化 Co-Cr 合金的金属-陶瓷结合强度。

Metal-ceramic bond strength of Co-Cr alloy fabricated by selective laser melting.

机构信息

Department of Prosthodontics, Ninth People's Hospital, Shanghai Jiao Tong University School of Medicine, Shanghai Key Laboratory of Stomatology, Shanghai, China.

出版信息

J Dent. 2012 Jun;40(6):453-7. doi: 10.1016/j.jdent.2012.02.006. Epub 2012 Mar 5.

Abstract

OBJECTIVES

This study was to evaluated the metal-ceramic bond strength of a Co-Cr dental alloy prepared using a selective laser melting (SLM) technique.

METHODS

Two groups comprised of twenty Co-Cr metal bars each were prepared using either a SLM or traditional lost-wax casting method. Ten bars from each group were moulded into standard ISO 9693:1999 dimensions of 25 mm × 3 mm × 0.5 mm with 1.1 mm of porcelain fused onto an 8 mm × 3 mm rectangular area in the centre of each bar. Metal-ceramic bonding was assessed using a three-point bending test. Fracture mode analysis and area fraction of adherence porcelain (AFAP) were determined by measuring Si content of specimens by SEM/EDS.

RESULTS

Student's t-test within the groups demonstrated no significant difference for the mean bond strength between the SLM and traditional cast sample groups. While SEM/EDS analysis indicated a mixed fracture mode on the debonding interface of both the SLM and the cast groups, the SLM group showed significantly more porcelain adherence than the control group (p<0.05).

CONCLUSIONS

The SLM metal-ceramic system exhibited a bonding strength that exceeds the requirement of ISO 9691:1999(E) and it even showed a better behaviour in porcelain adherence test comparable to traditional cast methods.

摘要

目的

本研究旨在评估采用选择性激光熔化(SLM)技术制备的 Co-Cr 牙科合金的金属-陶瓷结合强度。

方法

采用 SLM 或传统失蜡铸造方法各制备 20 根 Co-Cr 金属棒。每组的 10 根棒模制成符合 ISO 9693:1999 标准的尺寸,25mm×3mm×0.5mm,在每个棒的中心 8mm×3mm 的矩形区域上熔覆 1.1mm 的瓷。使用三点弯曲试验评估金属-陶瓷结合强度。通过 SEM/EDS 测量试样的 Si 含量,对断裂模式分析和附着瓷的面积分数(AFAP)进行了测定。

结果

组内学生 t 检验表明,SLM 和传统铸造样品组之间的平均结合强度没有显著差异。虽然 SEM/EDS 分析表明在 SLM 和铸造组的脱粘界面上均出现混合断裂模式,但 SLM 组的瓷附着量明显高于对照组(p<0.05)。

结论

SLM 金属-陶瓷系统表现出的结合强度超过 ISO 9691:1999(E)的要求,其在与传统铸造方法相当的瓷附着试验中表现出更好的性能。

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