Huang Jen-Ching, Li Chia-Lin, Lee Jyh-Wei
Department of Mechanical Engineering, Tungnan University, New Taipei City, Taiwan.
Scanning. 2012 Jan-Feb;34(1):51-9. doi: 10.1002/sca.20280. Epub 2011 Aug 24.
In this study, nanoscratching and nanomachining were conducted using an atomic force microscope (AFM) equipped with a doped diamond-coated probe (DDESP-10; VEECO) to evaluate the fabrication of nanopatterns on hard, Cr₂N/Cu multilayer thin films. The influence of normal force, scratch speed, and repeated scratches on the properties of hard multilayer thin films was also investigated. The nanoscratch experiments led researchers to establish a probe preparation and selection criteria (PPS criteria) to enhance the stability and accuracy of machining hard materials. Experimental results indicate that the depth of grooves produced by nanoscratching increased with an increase in normal force, while an increase in the number of scratches in a single location increased the groove depth but decreased friction. Therelationships among normal force and groove depth more closely resembled a logarithmic form than other mathematical models, as did the relationship between repeated scratching and its effect on groove depth and friction. The influence of scratch speed on friction was divided into two ranges. Between 0.1 and 2 µm/s, friction decreased logarithmically with an increase in scratch speed; however, when the speed exceeded 2 µm/s, the friction appeared stable. In this study, multilayered coatings were successfully machined, demonstrating considerable promise for the fabrication of nanopatterns in multilayered coatings at the nanoscale.
在本研究中,使用配备掺杂金刚石涂层探针(DDESP - 10;Veeco公司)的原子力显微镜(AFM)进行纳米划痕和纳米加工,以评估在硬Cr₂N/Cu多层薄膜上制备纳米图案的情况。还研究了法向力、划痕速度和重复划痕对硬多层薄膜性能的影响。纳米划痕实验促使研究人员建立了探针制备和选择标准(PPS标准),以提高加工硬质材料的稳定性和准确性。实验结果表明,纳米划痕产生的沟槽深度随法向力的增加而增加,而在单个位置划痕次数的增加会增加沟槽深度但降低摩擦力。法向力与沟槽深度之间的关系比其他数学模型更接近对数形式,重复划痕及其对沟槽深度和摩擦力的影响之间的关系也是如此。划痕速度对摩擦力的影响分为两个范围。在0.1至2 µm/s之间,摩擦力随划痕速度的增加呈对数下降;然而,当速度超过2 µm/s时,摩擦力趋于稳定。在本研究中,多层涂层成功加工,这表明在纳米尺度上在多层涂层中制备纳米图案具有很大的前景。