Fang X C, Yu B Y, Xiang B R, An D K
Department of Pharmaceutical Analysis, China Pharmaceutical University, Nanjing.
J Chromatogr. 1990 Aug 29;514(2):287-92. doi: 10.1016/s0021-9673(01)89400-0.
Pyrolysis-high-resolution gas chromatography-pattern recognition (Py-HRGC-PaRe) was used to develop a potential technique for identifying the Chinese traditional medicine Mai Dong. About 1 mg of crude drug powder was pyrolysed in a furnace pyrolyser and the products were directly carried into a gas chromatograph with an FSOT capillary column (30 m x 0.265 mm I.D.) coated with DB-1701 (df 0.25 micron). The Py-HRGC data were analysed by non-linear mapping PaRe. The results showed that Mai Dong samples could be classified into two categories: Ophiopogon japonicus (L.f.) Ker-Gawl (included in the Chinese Pharmacopoeia) and Liriope spicata.
热解-高分辨率气相色谱-模式识别(Py-HRGC-PaRe)被用于开发一种鉴别中药麦冬的潜在技术。约1毫克的药材粉末在炉式热解器中进行热解,产物直接导入配有FSOT毛细管柱(30米×0.265毫米内径)的气相色谱仪中,该毛细管柱涂覆有DB-1701(液膜厚度0.25微米)。通过非线性映射模式识别对Py-HRGC数据进行分析。结果表明,麦冬样品可分为两类:麦冬(《中国药典》收录)和山麦冬。