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2-氯-3-[(E)-(肼-1-基亚甲基)甲基]-6-甲氧基喹啉

2-Chloro-3-[(E)-(hydrazin-1-yl-idene)meth-yl]-6-meth-oxy-quinoline.

作者信息

Bouacida Sofiane, Bouraiou Abdelmalek, Benhamoud Nassima, Roisnel Thierry, Belfaitah Ali

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 May 1;68(Pt 5):o1548. doi: 10.1107/S1600536812017977. Epub 2012 Apr 28.

DOI:10.1107/S1600536812017977
PMID:22590409
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3344647/
Abstract

In the title compound, C(11)H(10)ClN(3)O, the quinoline ring system is essentially planar, the r.m.s. deviation for the non-H atoms being 0.014 (2) Å with a maximum deviation from the mean plane of 0.0206 (14) Å for the C atom bonded to the -CH-N=NH(2) group. In the crystal, molecules are linked via N-H⋯O and N-H⋯N hydrogen bonds, forming zigzag layers parallel to (010).

摘要

在标题化合物C₁₁H₁₀ClN₃O中，喹啉环系基本呈平面状，非氢原子的均方根偏差为0.014 (2) Å，与-CH-N=NH₂基团相连的C原子偏离平均平面的最大偏差为0.0206 (14) Å。在晶体中，分子通过N-H⋯O和N-H⋯N氢键相连，形成平行于(010)的锯齿状层。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6b3f/3344647/d64147108459/e-68-o1548-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6b3f/3344647/548fe70364c9/e-68-o1548-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6b3f/3344647/d64147108459/e-68-o1548-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6b3f/3344647/548fe70364c9/e-68-o1548-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6b3f/3344647/d64147108459/e-68-o1548-fig2.jpg

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本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2011 Aug 1;67(Pt 8):o2084-5. doi: 10.1107/S1600536811028170. Epub 2011 Jul 23.
2
The diastereoisomers 2-[(S/R)-2-chloro-3-quinolyl]-2-[(R)-1-(4-methoxyphenyl)ethylamino]acetonitrile at 100 K.非对映异构体2-[(S/R)-2-氯-3-喹啉基]-2-[(R)-1-(4-甲氧基苯基)乙氨基]乙腈，温度为100 K。
Acta Crystallogr C. 2009 Sep;65(Pt 9):o475-8. doi: 10.1107/S010827010903193X. Epub 2009 Aug 22.
3
A short history of SHELX.
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Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.