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3,6-二碘-9H-咔唑

3,6-Diiodo-9H-carbazole.

作者信息

Xie Yu-Zhong, Jin Jing-Yi, Jin Guang-De

机构信息

Department of Chemistry, Yanbian University, Yanji Jilin 133002, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Apr 1;68(Pt 4):o1242. doi: 10.1107/S1600536812012901. Epub 2012 Mar 31.

DOI:10.1107/S1600536812012901
PMID:22606175
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3344172/
Abstract

In the title compound, C(12)H(7)I(2)N, the tricyclic aromatic ring system is essentially planar, with an r.m.s. deviation of 0.0272 Å. The two I atoms are marginally out of plane, with the C-I bonds angled at 3.9 (2) and 1.1 (2)° with respect to the planes of their respective benzene rings, above and below the plane of the carbazole ring system. No classical hydrogen bonds are observed in the crystal structure.

摘要

在标题化合物C(12)H(7)I(2)N中，三环芳香环系基本呈平面状，均方根偏差为0.0272 Å。两个碘原子略微偏离平面，C-I键相对于各自苯环的平面分别在咔唑环系平面上方和下方呈3.9(2)°和1.1(2)°的角度。在晶体结构中未观察到经典氢键。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/852b/3344172/0e1e184c4d90/e-68-o1242-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/852b/3344172/0e1e184c4d90/e-68-o1242-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/852b/3344172/0e1e184c4d90/e-68-o1242-fig1.jpg

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