Nakamura Keisuke, Adolfsson Erik, Milleding Percy, Kanno Taro, Örtengren Ulf
Laboratory for Redox Regulation, Tohoku University Graduate School of Dentistry, Sendai, Japan.
Eur J Oral Sci. 2012 Jun;120(3):249-54. doi: 10.1111/j.1600-0722.2012.00958.x.
The aim of the present investigation was to study the influence of grain size on the strength of yttria-stabilized zirconia upon exposure to an additional heat treatment, mimicking the veneering process. The green bodies of zirconia discs prepared by cold isostatic pressing were sintered at 1,425, 1,500, or 1,575°C to customize the grain size. The disc-shaped specimens were highly polished and then processed with or without additional heat treatments (five times at 850-930°C). Ten specimens from each treatment group were subjected to a biaxial flexural strength test according to the ISO 6872 standard. The grain size of the specimens was analyzed by the mean linear intercept technique using scanning electron microscopy. It was demonstrated that the mechanical strength of zirconia ceramics was not reduced by the veneer firing processes when polished specimens were used, but the strength was found to decrease with increasing grain size. The raw materials and the sintering process used should be selected appropriately to avoid grain coarsening because it was found that the strength was influenced by large grains.
本研究的目的是研究晶粒尺寸对氧化钇稳定氧化锆强度的影响,该氧化锆在模拟贴面工艺的额外热处理后。通过冷等静压制备的氧化锆圆盘生坯在1425、1500或1575°C下烧结以定制晶粒尺寸。将圆盘形试样高度抛光,然后进行或不进行额外的热处理(在850 - 930°C下处理五次)。根据ISO 6872标准,对每个处理组的十个试样进行双轴弯曲强度测试。使用扫描电子显微镜通过平均线性截距技术分析试样的晶粒尺寸。结果表明,当使用抛光试样时,氧化锆陶瓷的机械强度不会因贴面烧制工艺而降低,但发现强度会随着晶粒尺寸的增加而降低。应适当选择所用的原材料和烧结工艺以避免晶粒粗化,因为发现强度受大晶粒的影响。