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[锡对大鼠的影响。1. 生物材料中铅存在下锡的萃取后反向伏安测定法]

[Effect of tin on rats. 1. Inverse voltammetric determination of tin in the presence of lead in biological material after extraction].

作者信息

Woggon H, Raab M, Jehle D

出版信息

Nahrung. 1979;23(5):561-6. doi: 10.1002/food.19790230511.

DOI:10.1002/food.19790230511
PMID:226887
Abstract

By means of inverse polarography, the authors determined tin selectively after double extraction with diethylammonium diethyl dithiocarbamate (DADDTC) in perchloric solution. The recovery rates were: in potatoes, 91.7 +/- 5.8%; in beef kidney, 85.0 +/- 22.7%; in beef liver 79.9 +/- 13.8%; and in milk, 69.8 +/- 11.4%. Possible interferences from other elements with the tin determination are discussed.

摘要

作者通过反向极谱法,在高氯酸溶液中用二乙基二硫代氨基甲酸二乙铵(DADDTC)进行两次萃取后选择性地测定锡。回收率分别为:土豆中91.7±5.8%;牛肾中85.0±22.7%;牛肝中79.9±13.8%;牛奶中69.8±11.4%。文中讨论了其他元素对锡测定可能产生的干扰。

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