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[雪松松针二氯甲烷提取物的化学成分研究]

[Study on the chemical constituent from the dichloromethane extract. of the pine needles of Cedrus deodara].

作者信息

Shi Xiao-Feng, Bai Zhao-Hui, Liu Dong-Yan, Li Shuang

机构信息

Gansu Academy of Medical Science, Lanzhou 730050, China.

出版信息

Zhong Yao Cai. 2012 Mar;35(3):404-6.

Abstract

OBJECTIVE

To study the chemical constituents of the dichloromethane extracted from pine needles of Cedrus deodara.

METHODS

Compounds were isolated and purified from the dichloromethane extract of pine needles by chromatography on silica gel and Sephadex LH-20. Their structures were identified on the basis of spectroscopic analysis and physicochemical property.

RESULTS

Nine compounds were isolated and purified. Their structures were identified as stigmasterol (1), oleanolic acid (2), parahydroxybenzaldehyde (3), beta-sitosterol (4), syringaresinol (5), daucosterol (6), p-hydroxybenzoic acid (7), gallicin (8) and gallic acid (9).

CONCLUSION

Compounds 1-3, 5 -9 are isolated from pine needles of this genus for the first time.

摘要

目的

研究喜马拉雅雪松松针二氯甲烷提取物的化学成分。

方法

通过硅胶柱色谱和葡聚糖凝胶LH - 20柱色谱从松针二氯甲烷提取物中分离纯化化合物,并根据光谱分析和理化性质鉴定其结构。

结果

分离并纯化出9种化合物,其结构分别鉴定为豆甾醇(1)、齐墩果酸(2)、对羟基苯甲醛(3)、β-谷甾醇(4)、丁香树脂醇(5)、胡萝卜苷(6)、对羟基苯甲酸(7)、没食子儿茶素(8)和没食子酸(9)。

结论

化合物1 - 3、5 - 9首次从该属松针中分离得到。

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