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[2,7-二甲氧基-8-(4-丙基苯甲酰基)萘-1-基](4-丙基苯基)甲酮

[2,7-Dimeth-oxy-8-(4-propyl-benzo-yl)naphthalen-1-yl](4-propyl-phen-yl)methanone.

作者信息

Sasagawa Kosuke, Hijikata Daichi, Sakamoto Rei, Okamoto Akiko, Yonezawa Noriyuki

机构信息

Department of Organic and Polymer Materials Chemistry, Tokyo University of Agriculture & Technology, Koganei, Tokyo 184-8588, Japan.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2596. doi: 10.1107/S1600536812033582. Epub 2012 Jul 28.

DOI:10.1107/S1600536812033582
PMID:22905019
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3415032/
Abstract

In the title compound, C(32)H(32)O(4), the 4-propyl-benzoyl groups at the 1- and 8-positions of the naphthalene ring system are aligned almost anti-parallel, and their benzene rings make a dihedral angle of 8.64 (10)°. The dihedral angles between the naphthalene ring system and the benzene rings are 69.37 (8) and 69.45 (8)°. In the crystal, C-H⋯O inter-actions link adjacent mol-ecules via their aroyl groups.

摘要

在标题化合物C(32)H(32)O(4)中，萘环体系1-位和8-位的4-丙基苯甲酰基几乎呈反平行排列，它们的苯环形成的二面角为8.64 (10)°。萘环体系与苯环之间的二面角分别为69.37 (8)°和69.45 (8)°。在晶体中，C—H⋯O相互作用通过其芳酰基连接相邻分子。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0d34/3415032/731b01ffdf8d/e-68-o2596-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0d34/3415032/20fc4fbdb07f/e-68-o2596-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0d34/3415032/731b01ffdf8d/e-68-o2596-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0d34/3415032/20fc4fbdb07f/e-68-o2596-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0d34/3415032/731b01ffdf8d/e-68-o2596-fig2.jpg

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本文引用的文献

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4-{[8-(4-Acetyl-oxybenzo-yl)-2,7-dimeth-oxy-naphthalen-1-yl]carbon-yl}phenyl acetate.4-{[8-(4-乙酰氧基苯甲酰基)-2,7-二甲氧基萘-1-基]羰基}苯基乙酸酯
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2503. doi: 10.1107/S160053681203228X. Epub 2012 Jul 21.
2
[8-(4-But-oxy-benzo-yl)-2,7-dimeth-oxy-naphthalen-1-yl](4-but-oxy-phen-yl)methanone.[8-(4-丁氧基-苯甲酰基)-2,7-二甲氧基-萘-1-基](4-丁氧基-苯基)甲酮
Acta Crystallogr Sect E Struct Rep Online. 2011 Dec 1;67(Pt 12):o3354. doi: 10.1107/S1600536811048550. Epub 2011 Nov 19.
3
{8-[4-(Bromo-meth-yl)benzo-yl]-2,7-dimeth-oxy-naphthalen-1-yl}[4-(bromo-meth-yl)phen-yl]methanone.
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