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利用聚焦连续切片的三维傅里叶变换评估低电压 TEM 性能。

Assessment of lower-voltage TEM performance using 3D Fourier transform of through-focus series.

机构信息

National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044, Japan.

出版信息

Ultramicroscopy. 2012 Oct;121:31-7. doi: 10.1016/j.ultramic.2012.06.012. Epub 2012 Jun 26.

Abstract

We assess the imaging performance of a transmission electron microscopy (TEM) system operated at a relatively low acceleration voltage using the three-dimensional (3D) Fourier transform of through-focus images. Although a single diffractogram and the Thon diagram cannot distinguish between the linear and non-linear TEM imaging terms, the 3D Fourier transform allows us to evaluate linear imaging terms, resulting in a conclusive assessment of TEM performance. Using this method, information transfer up to 98 pm is demonstrated for an 80 kV TEM system equipped with a spherical aberration corrector and a monochromator. We also revisit the Young fringe method in the light of the 3D Fourier transform, and have found a considerable amount of non-linear terms in Young fringes at 80 kV even from a typical standard specimen, such as an amorphous Ge thin film.

摘要

我们使用聚焦差图像的三维(3D)傅里叶变换来评估在相对低的加速电压下运行的透射电子显微镜(TEM)系统的成像性能。虽然单个衍射线和 Thon 图不能区分线性和非线性 TEM 成像项,但 3D 傅里叶变换允许我们评估线性成像项,从而对 TEM 性能进行明确评估。使用这种方法,我们证明了配备有球差校正器和单色仪的 80kV TEM 系统的信息传递高达 98pm。我们还根据 3D 傅里叶变换重新考察了杨氏条纹法,即使对于典型的标准样品(如非晶 Ge 薄膜),我们也在 80kV 时发现了杨氏条纹中相当数量的非线性项。

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