IFW Dresden, PF 27 01 16, Dresden, Germany.
J Microsc. 2013 Feb;249(2):87-92. doi: 10.1111/j.1365-2818.2012.03684.x. Epub 2012 Nov 23.
For the characterization of light materials using transmission electron microscopy, a low electron acceleration voltage of 80 kV or even 60 kV is attractive due to reduced beam damage to the specimen. The concomitant reduction in resolving power of the microscope can be restored when using spherical aberration (C(s) ) correctors, which for the most part are only available in the latest and most expensive microscopes. Here, we show that upgrading of existing TEMs is an attractive and cost-effective alternative. We report on the low-voltage performance on graphitic material of a JEOL JEM-2010F built in the early 1990s and retro-fitted with a conventional imaging C(s) corrector and a probe C(s) corrector. The performance data show C(s) retro-fitted instruments can compete very favourably against more modern state-of-the-art instruments in both conventional imaging (TEM) and scanning (STEM) modes.
为了使用透射电子显微镜对轻材料进行表征,由于减少了对样品的电子束损伤,因此 80kV 甚至 60kV 的低电子加速电压很有吸引力。当使用球差(C(s))校正器时,可以恢复显微镜的分辨率,而这些校正器在大多数情况下仅在最新和最昂贵的显微镜中可用。在这里,我们表明,对现有 TEM 进行升级是一种有吸引力且具有成本效益的选择。我们报告了早在 1990 年代制造的 JEOL JEM-2010F 在经过改装配备常规成像 C(s)校正器和探针 C(s)校正器后对石墨材料的低电压性能。性能数据表明,配备 C(s)校正器的仪器在常规成像(TEM)和扫描(STEM)模式下都可以与更现代的最先进仪器非常有利地竞争。