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纳米纤维素纤维的制备及其在卡拉胶基膜中的应用。

Preparation of nano cellulose fibers and its application in kappa-carrageenan based film.

机构信息

Department of Polymer and Surface Engineering, Institute of Chemical Technology, Matunga (E), Mumbai 400019, India.

出版信息

Int J Biol Macromol. 2012 Dec;51(5):1008-13. doi: 10.1016/j.ijbiomac.2012.08.014. Epub 2012 Aug 24.

Abstract

Bio-based nanocomposite films were successfully developed using nanofibrillated cellulose (NFC) as the reinforcing phase and kappa-carrageenan (KCRG) as the matrix. NFC was successfully synthesis from short stable cotton fibers by chemo-mechanical process. The bionanocomposites were prepared by incorporating 0.1, 0.2, 0.3, 0.4, 0.5, and 1wt% of the NFC into a KCRG matrix using a solution casting method there characterization was done in terms of thermal properties (DSC), morphology (SEM), water vapor transmission rate (WVTR), oxygen transmission rate (OTR), X-ray diffractograms (XRD), and tensile properties. The main conclusion arising from the analysis of the result is that the bionanocomposites containing 0.4wt% of NFC exhibited the highest enhancement in tensile strength it is almost 44% improvement. WVTR and OTR results showed improvement of all nanocomposite film compare to control KCRG film.

摘要

采用纳米原纤化纤维素(NFC)作为增强相和角叉菜胶(KCRG)作为基质,成功制备了生物基纳米复合材料薄膜。NFC 是通过化学机械法从短稳棉花纤维中成功合成的。通过溶液浇铸法将 0.1、0.2、0.3、0.4、0.5 和 1wt%的 NFC 掺入 KCRG 基质中,制备了生物纳米复合材料,并对其进行了热性能(DSC)、形貌(SEM)、水蒸气透过率(WVTR)、氧气透过率(OTR)、X 射线衍射图(XRD)和拉伸性能的分析。从结果分析中得出的主要结论是,含有 0.4wt%NFC 的生物纳米复合材料表现出最高的拉伸强度增强,几乎提高了 44%。WVTR 和 OTR 结果表明,与对照 KCRG 薄膜相比,所有纳米复合材料薄膜的性能都得到了改善。

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