Biomaterials Unit, University of Birmingham, School of Dentistry, College of Medical and Dental Sciences, St. Chads Queensway, Birmingham B4 6NN, United Kingdom.
Dent Mater. 2012 Nov;28(11):1154-61. doi: 10.1016/j.dental.2012.08.010. Epub 2012 Sep 1.
To test the influence of specimen dimensions on light transmission and shrinkage strain properties of curing dental resins.
Photocurable resin specimens (Bis-GMA/TEGDMA) with aspect ratios (AR) of 2 (4mm×2mm); 4 (4mm×1mm and 8mm×2mm); 8 (8mm×1mm); 12 (AR: 12mm×1mm); and 24 (12mm×0.5mm) were light cured. Light transmission and shrinkage-strain data were recorded throughout, and upper and lower surface hardness measurements were performed following cure.
Light transmission was significantly affected by the specimen aspect ratio even at similar thicknesses (p<0.05). By comparing light transmission through a negative control resin without photoinitiator, the lowest AR specimens showed a relative increase in transmission above 100% throughout curing, which was caused by specimen constraint. The extent of lower surface cure (as assessed by increasing hardness) was principally affected by cavity height and decreased for thicker specimens (p<0.05). Only the 2mm thick specimens showed a significantly greater lower to upper hardness ratio with increasing cavity diameter (p<0.05). The highest AR specimen showed the greatest lower to upper hardness percentage (p<0.05), and was expected since this AR was obtained by reducing the sample thickness to 0.5mm. Generally, total shrinkage strain increased and shrinkage strain per unit mass decreased with increasing AR.
Specimen constraint in low AR cavities may compromise light transmission as unexpected light intensity variations may occur for low configuration factors, which ultimately affect polymer conversion of light-cured resin-based restorations through depth.
测试试件尺寸对固化牙科树脂透光率和收缩应变性能的影响。
将具有纵横比(AR)为 2(4mm×2mm);4(4mm×1mm 和 8mm×2mm);8(8mm×1mm);12(AR:12mm×1mm);和 24(12mm×0.5mm)的光固化可聚合树脂试件(Bis-GMA/TEGDMA)进行光固化。记录整个过程中的透光率和收缩应变数据,并在固化后进行上下表面硬度测量。
即使在相似厚度下,试件纵横比也会显著影响透光率(p<0.05)。通过比较无光引发剂的负对照树脂的透光率,最低 AR 试件在整个固化过程中显示出相对透光率增加超过 100%,这是由试件约束引起的。下部表面固化程度(通过增加硬度来评估)主要受腔深影响,并且对于较厚的试件减小(p<0.05)。仅 2mm 厚的试件显示出随着腔直径增加而显著更大的下至上硬度比(p<0.05)。最高 AR 试件显示出最大的下至上硬度百分比(p<0.05),这是预期的,因为该 AR 通过将样品厚度减小到 0.5mm 获得。通常,随着 AR 的增加,总收缩应变增加,单位质量的收缩应变减小。
低 AR 腔中的试件约束可能会影响透光率,因为低配置因子可能会出现意想不到的光强变化,这最终会影响通过深度的光固化树脂基修复体的聚合物转化率。