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采用不会导致结果偏低的HNO₃/HClO₃/HClO₄消解方法测定鱼类中的总汞(作者译)

[Determination of total mercury in fish by means of a digestion method with HNO3/HClO3/HClO4 which does not lead to low results (author's transl)].

作者信息

Kruse R

出版信息

Z Lebensm Unters Forsch. 1979 Oct;169(4):259-62. doi: 10.1007/BF01193790.

Abstract

A digestion method for determination of total mercury in fish is described, which is economical, simple and reliable. Digestion is carried out by wet ashing with HNO3/HClO3/HClO4 in the presence of chloric acid. The procedure can be carried out at normal pressure in test tubes without suffering losses of Hg. The determination itself is carried out by the well known cold vapor atomic absorption method. This method was worked out specially for the regulatory control of fish, but can probably be used for related problems.

摘要

本文描述了一种用于测定鱼类总汞含量的消化方法,该方法经济、简便且可靠。消化过程采用在氯酸存在下用硝酸/高氯酸/高氯酸进行湿式灰化。该操作可在试管中常压下进行,汞不会损失。测定本身采用众所周知的冷蒸气原子吸收法进行。该方法是专门为鱼类的监管控制而制定的,但可能也适用于相关问题。

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