Mechanical properties of controlled memory and superelastic nickel-titanium wires used in the manufacture of rotary endodontic instruments.

INTRODUCTION

The aim of this study was to investigate the structure and mechanical properties of newly developed controlled memory (CM) nickel-titanium wires used in the manufacture of rotary endodontic instruments.

METHODS

The composition and the phase transformation behavior of both types of wires were examined by x-ray energy dispersive spectroscopy and differential scanning calorimetry, respectively. Conventional superelastic (SE) nickel-titanium wire was used as a control. The mechanical properties of the wires at selected temperatures (room temperature, 37°C, and 60°C) were evaluated with tensile, cyclic tensile, and cantilever bending tests by using an Instron 3365 universal testing machine. The data of austenitic transformation finishing temperature (A(f)) were analyzed statistically by using 1-way analysis of variance test at a significance level of P < .05.

RESULTS

The raw CM wires contained a nickel content of 50.7% ± 0.5% and possessed a relatively higher A(f) than SE wires (P < .05). The critical plateau stress and ultimate tensile strength of the CM wires were lower than they were for the SE wires, but the maximum strain before fracture of the CM wires (58.4% ± 7.5% to 84.7% ± 6.8%) was more than 3 times higher than it was for SE wires (16.7% ± 3.8% to 27.5% ± 5.4%). The maximum strain of the CM wires with a diameter of 1.22 mm tested at room temperature (23°C ± 2°C) was up to 84% ± 6.4%. CM wires were not SE at either room temperature or 37°C; however, they exhibited superelasticity when heated to 60°C.

CONCLUSIONS

The raw CM wires exhibited different phase transformation behavior and mechanical properties when compared with SE wires, attributing to the special heat treatment history of CM wires. This study suggested greater flexibility of endodontic instruments manufactured with CM wires than similar instruments made of conventional SE wires.