Alves Paula Barbosa, Brandt William Cunha, Neves Ana Christina Claro, Cunha Leonardo Gonçalves, Silva-Concilio Lais Regiane
Department of Prosthodontics, Dentistry School, University of Taubate, Taubate-SP, BRAZIL.
Eur J Dent. 2013 Jan;7(1):117-22.
The objective of this study was to evaluate the diametral tensile strength (DTS) and Knoop hardness (KH) of direct (Filtek Z350-3M/ESPE and Charisma-Heraeus Kulzer) and indirect composites (Sinfony-3M/ESPE and Signum-Heraeus Kulzer) kept in storage for two periods of time, 24 hours and 10 months, in distilled water.
Twenty-five specimens of each material were prepared. DTS (n=10) was tested using a universal testing machine (Versat, model 2000) at a crosshead speed of 1.0 mm/min. KH (n=5) was measured using Knoop micro-hardness (HMV-2000; 50 gf for 15 s). All tests were performed 24 hours after polymerization and after 10 months of storage in distilled water at 37°C. The data were statistically analyzed using Kolmogorov-Smirnov, ANOVA and t-Student (P=.05).
Filtek Z350, Sinfony, and Signum showed higher DTS values than Charisma after 24 hours. After storage, Sinfony and Signum showed higher DTS values because the storage did not influence the DTS values of the indirect composites. Filtek Z350 showed higher KH values after 24 hours and after storage than other composites; the storage influenced the KH of all composites except Sinfony.
Storage for 10 months did not influence the properties of the indirect composite Sinfony. In general, the indirect composites showed higher DTS values than direct composites, especially after 10 months storage. The direct composite Filtek Z350 obtained the highest KH values regardless of storage.
本研究的目的是评估直接复合材料(Filtek Z350 - 3M/ESPE和Charisma - Heraeus Kulzer)和间接复合材料(Sinfony - 3M/ESPE和Signum - Heraeus Kulzer)在蒸馏水中储存24小时和10个月这两个时间段后的径向拉伸强度(DTS)和努氏硬度(KH)。
每种材料制备25个样本。使用万能试验机(Versat,型号2000)以1.0 mm/min的十字头速度测试DTS(n = 10)。使用努氏显微硬度计(HMV - 2000;50 gf,保持15秒)测量KH(n = 5)。所有测试均在聚合24小时后以及在37°C蒸馏水中储存10个月后进行。使用Kolmogorov - Smirnov、方差分析和t检验对数据进行统计学分析(P = 0.05)。
24小时后,Filtek Z350、Sinfony和Signum的DTS值高于Charisma。储存后,Sinfony和Signum的DTS值更高,因为储存不影响间接复合材料的DTS值。24小时后及储存后,Filtek Z350的KH值高于其他复合材料;储存影响了除Sinfony之外的所有复合材料的KH。
储存10个月不影响间接复合材料Sinfony的性能。总体而言,间接复合材料的DTS值高于直接复合材料,尤其是在储存10个月后。直接复合材料Filtek Z350无论是否储存都获得了最高的KH值。