改进的玉米赤霉烯酮和串珠镰刀菌素的制备方法。
Improved methods of zearalenone and moniliformin preparation.
机构信息
Department of Chemistry, Agricultural University, ul. Wojska Polskiego 75, 60-625, Poznań, Poland.
出版信息
Mycotoxin Res. 1987 Mar;3 Suppl 1:61-4. doi: 10.1007/BF03192030.
PMID:23605022
Abstract
Modified procedures of zearalenone and moniliformin preparation, using solid substrate (rice or corn kernels) has been developed. Preliminary purification of toxins by 1iquid-liquid partition was applied, followed by column chromatography on silicagel and charcoal. Final yield was about lg from 1kg of dry cultures of crystalline zearalenone and liophylized moniliformin o high purity.
摘要
已开发出一种使用固体基质（大米或玉米粒）来制备玉米赤霉烯酮和串珠镰孢菌毒素的改良方法。采用液-液分配法对毒素进行初步纯化，然后用硅胶和活性炭进行柱层析。从 1 公斤结晶玉米赤霉烯酮和冻干高纯度串珠镰孢菌毒素的干燥培养物中，最终的产量约为 1 克。
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