蜜环菌菌丝体化学成分的研究。V. 蜜环菌素和蜜环菌宁的分离与表征
[Studies on the chemical constituents of Armillaria mellea mycelium. V. Isolation and characterization of armillarilin and armillarinin].
作者信息
Yang J S, Su Y L, Wang Y L, Feng X Z, Yu D Q, Liang X T
机构信息
Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing.
出版信息
Yao Xue Xue Bao. 1990;25(1):24-8.
Two new protoilludane sesquiterpenoid aromatic esters, armillarilin C24H30O7, mp 179-180 degrees C, [alpha]D14 + 162 (c 0.97 CHC1(3] and armillarinin C24H29O7 C1, mp 152-155 degrees C, [alpha]D17 + 153.6, (c 0.09, CHC1(3], have been isolated from the artifically cultured mycelium of Armillaria mellea (Vahl. ex Fr.) Quel (Tricholometaceae). On the basis of spectral (UV, IR, 1HNMR, 13CNMR and MS) analysis their structures were identified as I and II, respectively.
从蜜环菌（Armillaria mellea (Vahl. ex Fr.) Quel，口蘑科）的人工培养菌丝体中分离出两种新的原伊鲁烷倍半萜芳香酯，蜜环菌酯C24H30O7，熔点179 - 180℃，[α]D14 + 162（c 0.97，CHC1₃）和蜜环菌素C24H29O7 C1，熔点152 - 155℃，[α]D17 + 153.6（c 0.09，CHC1₃）。基于光谱（紫外、红外、¹H核磁共振、¹³C核磁共振和质谱）分析，它们的结构分别被鉴定为I和II。
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