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用高浓度漂白剂蚀刻纤维桩表面。

Etching a fiber post surface with high-concentration bleaching agents.

作者信息

Menezes M S, Faria-e-Silva A L, Silva F P, Reis G R, Soares C J, Stape T H S, Martins L R

出版信息

Oper Dent. 2014 Jan-Feb;39(1):E16-21. doi: 10.2341/12-270-L. Epub 2013 Jul 12.

Abstract

INTRODUCTION

Commonly, resin composites/cements fail to achieve proper bonding to fiber posts when their surfaces have not been previously etched. This study evaluated the effect of the concentration and application mode of hydrogen peroxide on the surface topography and bond strength of resin composite to glass-fiber posts.

METHODS AND MATERIALS

Fiber posts were immersed in 24% or 35% solutions (a high-concentration bleaching agent) of hydrogen peroxide (H2O2), or these solutions were applied over the post surface using a microbrush (n=10). Posts without any treatment were used as a control. After etching, the posts were silanated and an adhesive was applied. The posts were positioned in a mold, and a resin composite was incrementally inserted and light-cured. The post/resin assembly was serially sectioned into several beams that were subjected to a tensile bond strength test. The data were subjected to the two-way analysis of variance and Tukey test (α=0.05). The Dunnet's test was used to compare the experimental conditions to the control. The surface topography was analyzed using scanning electronic microscopy.

RESULTS

The non-etched post presented a relatively smooth surface without fiber exposure. Except for the application of 24% H2O2, the other experimental conditions increased the number of exposed fibers and bond strength in relation to the control. Although immersion resulted in higher values for the 24% H2O2 application, the mode of application did not alter bond strength when 35% H2O2 was used.

CONCLUSIONS

The effect of the mode of application of H2O2 depended on its level of concentration. A high-concentration bleaching agent improved the bond strength of the resin composite to the post surface, regardless of which mode was used.

摘要

引言

通常情况下,当树脂复合材料/粘结剂的表面未预先蚀刻时,它们无法与纤维桩实现良好的粘结。本研究评估了过氧化氢的浓度和应用方式对树脂复合材料与玻璃纤维桩表面形貌及粘结强度的影响。

方法与材料

将纤维桩浸入24%或35%的过氧化氢(H2O2)溶液(一种高浓度漂白剂)中,或者用微型刷将这些溶液涂抹在桩表面(n = 10)。未进行任何处理的桩用作对照。蚀刻后,对桩进行硅烷化处理并施加粘结剂。将桩放置在模具中,逐步插入树脂复合材料并进行光固化。将桩/树脂组件依次切成几根梁,进行拉伸粘结强度测试。数据进行双向方差分析和Tukey检验(α = 0.05)。使用Dunnet检验将实验条件与对照进行比较。使用扫描电子显微镜分析表面形貌。

结果

未蚀刻的桩表面相对光滑,没有纤维暴露。除了使用24% H2O2外,其他实验条件与对照相比增加了暴露纤维的数量和粘结强度。尽管浸入法在使用24% H2O2时得到的值更高,但在使用35% H2O2时,应用方式并未改变粘结强度。

结论

过氧化氢的应用方式的影响取决于其浓度水平。无论使用哪种方式,高浓度漂白剂都能提高树脂复合材料与桩表面的粘结强度。

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