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微波/实验室光源后固化技术及湿老化对复合树脂显微硬度的影响

The effect of microwave/laboratory light source postcuring technique and wet-aging on microhardness of composite resin.

作者信息

Sharafeddin Farahnaz, Sharifi Elham

机构信息

Department of Operative Dentistry, Specialist in Operative Dentistry, Biomaterial Research Center, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

出版信息

Dent Res J (Isfahan). 2013 May;10(3):370-5.

Abstract

BACKGROUND

Although composite restorations are really valuable for esthetic zones, they have shown less longevity rather than amalgam restorations. Since it may be related to the method used for curing the composite, postcuring could increase the degree of conversion and result in more long-lasting composite restorations. This study was planned to evaluate the effect of two different postcuring techniques on microhardness of indirect composite resin after wet-aging and comparing them with the direct type.

MATERIALS AND METHODS

In this experimental study, 99 composite disk-shaped (6.5 × 2.5 mm) specimens of composite (Gradia GC, Japan) were prepared in split mold. The indirect composite specimens were postcured by laboratory light source (Labolite LV-III GC Corp, Japan) or microwave unit (MC 2002 JR, LG, Korea). Then, the aging procedure was done for 24 h, 30 and 180 days in distilled water. The Vicker's Hardness test (VHN) on surface of specmens was measured by Wolpert microhardness tester and the data were analyzed by the two-way analysis of variance (ANOVA) and Tukey's post hoc tests. (P ≤ 0.05).

RESULTS

The statistical analysis revealed that surface microhardness of postcured composite by microwave and laboratory light source was more than that of direct composite (P = 0.0001) and postcuring by microwave was more effective than postcuring by laboratory light source (P = 0.004). The 30 days stored composite demonstrated significant decrease of VHN compared with the 24-h stored samples (P = 0.0001), with a more significant VHN decrease after 180 days of aging (P = 0.045).

CONCLUSION

Postcuring increased the surface microhardness and aging reduced the surface microhardness of indirect composite.

摘要

背景

尽管复合树脂修复体对于美观区域非常有价值,但与汞合金修复体相比,其使用寿命较短。由于这可能与复合树脂的固化方法有关,二次固化可能会提高转化率,从而使复合树脂修复体更持久。本研究旨在评估两种不同的二次固化技术对间接复合树脂在湿老化后的显微硬度的影响,并将其与直接型复合树脂进行比较。

材料与方法

在本实验研究中,使用分体模具制备了99个复合树脂圆盘形(6.5×2.5mm)试件(日本GC公司的Gradia)。间接复合树脂试件通过实验室光源(日本GC公司的Labolite LV-III)或微波装置(韩国LG公司的MC 2002 JR)进行二次固化。然后,在蒸馏水中进行24小时、30天和180天的老化处理。使用Wolpert显微硬度计测量试件表面的维氏硬度(VHN),并通过双向方差分析(ANOVA)和Tukey事后检验对数据进行分析(P≤0.05)。

结果

统计分析表明,经微波和实验室光源二次固化的复合树脂的表面显微硬度高于直接复合树脂(P = 0.0001),且微波二次固化比实验室光源二次固化更有效(P = 0.004)。与储存24小时的样品相比,储存30天的复合树脂的VHN显著降低(P = 0.0001),老化180天后VHN降低更显著(P = 0.045)。

结论

二次固化提高了间接复合树脂的表面显微硬度,而老化降低了其表面显微硬度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6e0a/3760362/2e70714f97e6/DRJ-10-370-g001.jpg

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