Department of Chemistry, University of Science and Technology of China , Hefei 230026, P. R. China.
Langmuir. 2013 Oct 15;29(41):12818-22. doi: 10.1021/la402473k. Epub 2013 Oct 4.
ZnIn2S4 nanotubes and nanowires have been selectively fabricated via a convenient one-step wet-chemical approach by using porous polycarbonate membrane as a hard template. The wall of nanotubes is as thin as 5 nm, and the diameter of them is 200 nm. Formation mechanism of ZnIn2S4 nanotubes and nanowires is also discussed according to the experimental results. The structure, morphology, and composition properties of the as-prepared samples were characterized using X-ray powder diffraction, UV-vis spectrophotometer, transmission electron microscopy, energy dispersive X-ray spectrometry, and scanning electron microscopy.
ZnIn2S4 纳米管和纳米线已通过使用多孔聚碳酸酯膜作为硬模板的简便一步湿法化学方法被选择性地制造。纳米管的壁厚度薄至 5nm,直径为 200nm。还根据实验结果讨论了 ZnIn2S4 纳米管和纳米线的形成机制。使用 X 射线粉末衍射仪、紫外可见分光光度计、透射电子显微镜、能谱仪和扫描电子显微镜对制备样品的结构、形貌和组成特性进行了表征。