Department of Food Technology, Kongu Engineering College, Perundurai 638052, Erode, Tamilnadu, India.
Int J Biol Macromol. 2013 Nov;62:565-73. doi: 10.1016/j.ijbiomac.2013.09.027. Epub 2013 Sep 27.
The present study investigates the influence of composition (content of maize starch (1-3 g), sorbitol (0.5-1.0 ml), agar (0.5-1.0 g) and tween-80 (0.1-0.5 ml)) on the mechanical properties (tensile strength, elongation, Young's modulus, puncture force and puncture deformation) of the maize starch based edible films using four factors with three level Box-Behnken design. The edible films were obtained by casting method. The results showed that, tween-80 increases the permeation of sorbitol in to the polymer matrix. Increasing concentration of sorbitol (hydrophilic nature and plasticizing effect of sorbitol) decreases the tensile strength, Young's modulus and puncture force of the films. The results were analyzed by Pareto analysis of variance (ANOVA) and second order polynomial models were obtained for all responses with high R(2) values (R(2)>0.95). 3D response surface plots were constructed to study the relationship between process variables and the responses.
本研究采用四因素三水平 Box-Behnken 设计,考察了组成(1-3 g 玉米淀粉、0.5-1.0 ml 山梨糖醇、0.5-1.0 g 琼脂和 0.1-0.5 ml tween-80)对玉米淀粉基可食用膜力学性能(拉伸强度、伸长率、杨氏模量、穿刺力和穿刺变形)的影响。采用浇注法制备可食用膜。结果表明,tween-80 增加了山梨糖醇在聚合物基质中的渗透。山梨糖醇浓度的增加(山梨糖醇的亲水性和增塑作用)降低了薄膜的拉伸强度、杨氏模量和穿刺力。采用方差分析(ANOVA)对 Pareto 进行了分析,并得到了所有响应的二次多项式模型,R(2)值均较高(R(2)>0.95)。构建了 3D 响应面图来研究工艺变量与响应之间的关系。