Sun Hong-Shun, Li Yu-Long, Xu Ning, Xu Hong, Zhang Ji-Dong
Chemical Engineering Department, Nanjing College of Chemical Technology, Geguan Road No. 265 Nanjing, Nanjing 210048, People's Republic of China.
Acta Crystallogr Sect E Struct Rep Online. 2013 Sep 7;69(Pt 10):o1516. doi: 10.1107/S1600536813024471. eCollection 2013.
In the title compound, C27H22N2O4, the two indole ring systems are approximately perpendicular to each other, with a dihedral angle of 84.5 (5)° between their planes; the benzene ring is twisted with respect to the two indole ring systems at angles of 78.5 (5) and 86.5 (3)°. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds, weak C-H⋯O and C-H⋯N hydrogen bonds, and C-H⋯π inter-actions into a three-dimensional supra-molecular architecture.
在标题化合物C₂₇H₂₂N₂O₄中,两个吲哚环系统彼此大致垂直,它们的平面之间的二面角为84.5 (5)°;苯环相对于两个吲哚环系统扭转的角度分别为78.5 (5)°和86.5 (3)°。在晶体中,分子通过N-H⋯O氢键、弱C-H⋯O和C-H⋯N氢键以及C-H⋯π相互作用连接成三维超分子结构。