Zinelis Spiros, Sifakakis Iosif, Katsaros Christos, Eliades Theodore
*Biomaterials, and.
**Orthodontics, School of Dentistry, National and Kapodistrian University of Athens, Greece.
Eur J Orthod. 2014 Aug;36(4):389-93. doi: 10.1093/ejo/cjt086. Epub 2013 Nov 14.
To investigate the composition and the microstructural and mechanical characterization of three different types of lingual brackets.
Incognito™ (3M Unitek), In-Ovation L (DENTSPLY GAC) and STb™ (Light Lingual System, ORMCO) lingual brackets were studied under the scanning electron microscope employing backscattered electron imaging and their elemental composition was analysed by energy-dispersive X-ray microanalysis. Additionally, Vickers hardness was assessed using a universal hardness-testing machine, and the indentation modulus was measured according to instrumented indentation test. Two-way analysis of variance was conducted employing bracket type and location (base and wing) as discriminating variable. Significant differences among groups were allocated by post hoc Student-Newman-Keuls multiple comparison analysis at 95% level of significance.
Three different phases were identified for Incognito and In-Ovation L bracket based on mean atomic number contrast. On the contrary, STb did not show mean atomic contrast areas and thus it is recognized as a single phase. Incognito is a one-piece bracket with the same structure in wing and base regions. Incognito consists mainly of noble metals while In-Ovation L and STb show similar formulations of ferrous alloys in wing and base regions. No significant differences were found between ferrous brackets in hardness and modulus values, but there were significant differences between wing and base regions. Incognito illustrated intermediate values with significant differences from base and wing values of ferrous brackets.
CONCLUSIONS/IMPLICATIONS: Significant differences exist in microstructure, elemental composition, and mechanical properties among the brackets tested; these might have a series of clinical implications during mechanotherapy.
研究三种不同类型舌侧托槽的组成、微观结构及力学特性。
采用背散射电子成像技术,在扫描电子显微镜下对Incognito™(3M Unitek公司)、In - Ovation L(登士柏GAC公司)和STb™(ORMCO公司的Light Lingual System)舌侧托槽进行研究,并通过能量色散X射线微分析对其元素组成进行分析。此外,使用万能硬度测试机评估维氏硬度,并根据仪器化压痕试验测量压痕模量。以托槽类型和位置(基底和翼)作为区分变量进行双向方差分析。在95%显著性水平下,通过事后学生 - 纽曼 - 库尔斯多重比较分析确定组间的显著差异。
基于平均原子序数对比,在Incognito和In - Ovation L托槽中识别出三个不同相。相反,STb未显示平均原子对比区域,因此被认为是单相。Incognito是一种一体式托槽,在翼和基底区域具有相同结构。Incognito主要由贵金属组成,而In - Ovation L和STb在翼和基底区域显示出类似的铁合金配方。铁基托槽在硬度和模量值方面未发现显著差异,但翼和基底区域之间存在显著差异。Incognito显示出中间值,与铁基托槽的基底和翼值存在显著差异。
结论/启示:在所测试的托槽之间,微观结构、元素组成和力学性能存在显著差异;这些差异在机械治疗过程中可能具有一系列临床意义。