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原位 EBSD 在拉伸试验中的应用铝合金 AA3003 板材。

In situ EBSD during tensile test of aluminum AA3003 sheet.

机构信息

Division of Engineering Materials, Department of Management & Engineering, Linköping University, SE-58183 Linköping, Sweden; Gränges Technology, Gränges AB, SE-61281 Finspong, Sweden.

Division of Engineering Materials, Department of Management & Engineering, Linköping University, SE-58183 Linköping, Sweden.

出版信息

Micron. 2014 Mar;58:15-24. doi: 10.1016/j.micron.2013.11.001. Epub 2013 Nov 15.

Abstract

Miniature tensile-test specimens of soft-annealed, weakly textured AA3003 aluminum sheet in 0.9 mm thickness were deformed until fracture inside a scanning electron microscope. Tensile strength measured by the miniature tensile test stage agreed well with the tensile strength by regular tensile testing. Strain over the microscope field of view was determined from changes in positions of constituent particles. Slip lines were visible in secondary electron images already at 0.3% strain; activity from secondary slip systems became apparent at 2% strain. Orientation rotation behavior of the tensile load axis with respect to the crystallographic axes agreed well with previously reported trends for other aluminum alloys. Start of the fracture and tensile crack propagation were documented in secondary electron images. The region of fracture nucleation included and was surrounded by many grains that possessed high Schmid factors at zero strain. Crystal lattice rotation angles in the grains surrounding the initial fracture zone were higher than average while rotations inside the initial fracture zone were lower than average for strains from zero to 31%. The orientation rotation behavior of the tensile load axes of the grains around the fracture zone deviated from the average behavior in this material.

摘要

厚度为 0.9 毫米的软退火、弱织构 AA3003 铝合金的微型拉伸试验试样在扫描电子显微镜内变形直至断裂。微型拉伸试验台上测量的拉伸强度与常规拉伸试验的拉伸强度吻合良好。通过观察组成颗粒的位置变化来确定显微镜视场内的应变。在 0.3%应变时,在二次电子图像中已经可以看到滑移线;在 2%应变时,次级滑移系统的活动变得明显。拉伸载荷轴相对于晶体轴的取向旋转行为与其他铝合金的先前报道趋势吻合良好。在二次电子图像中记录了断裂的起始和拉伸裂纹的扩展。断裂核的形成区域包括并被许多在零应变时具有高施密特因子的晶粒包围。在初始断裂区周围的晶粒中,晶格旋转角高于平均值,而在初始断裂区内部,旋转角低于平均值,应变从 0 到 31%。断裂区周围晶粒的拉伸载荷轴的取向旋转行为偏离了该材料的平均行为。

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