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化学蚀刻颜色中的取向错误/局部塑性应变表现

Misorientation/local plastic strain manifestations in chemical etching color.

作者信息

Zhang Xianguang, Matsuura Kiyotaka, Ohno Munekazu

机构信息

Graduate School of Engineering, Hokkaido University, Kita 13, Nishi 8, Kita-ku, Sapporo, Hokkaido 060-8628, Japan.

Division of Materials Science and Engineering, Faculty of Engineering, Hokkaido University, Kita 13, Nishi 8, Kita-ku, Sapporo, Hokkaido 060-8628, Japan.

出版信息

Micron. 2014 Apr;59:28-32. doi: 10.1016/j.micron.2013.12.008. Epub 2013 Dec 24.

Abstract

Cold plastic deformation produces misorientations inside the crystal grains, and the distribution of the misorientation is quite crucial to understand the deformation behavior of the metals or alloys. The misorientation manifestations in chemical etching contrast are investigated in this study in the case of cold-deformed iron. The chemical etching is performed by using nital, while the crystal orientation is determined by electron backscatter diffraction (EBSD). The correlation between the chemical etching contrast and crystal orientation have been studied in both cold-deformed and undeformed iron. The results clearly show that the chemical etching contrast strongly reflects the crystallographic orientation. The gradual change in chemical etching contrast inside the individual deformed grains gives information of both the misorientation and local plastic strain within the grains. This method can provide an easy and alternative way to qualitatively understand the misorientation and local plastic strain distributions in the microstructures.

摘要

冷塑性变形会在晶粒内部产生取向差,而取向差的分布对于理解金属或合金的变形行为至关重要。本研究针对冷变形铁的情况,研究了化学蚀刻对比度中的取向差表现。使用硝酸酒精溶液进行化学蚀刻,同时通过电子背散射衍射(EBSD)确定晶体取向。研究了冷变形和未变形铁中化学蚀刻对比度与晶体取向之间的相关性。结果清楚地表明,化学蚀刻对比度强烈反映了晶体取向。单个变形晶粒内部化学蚀刻对比度的逐渐变化给出了晶粒内取向差和局部塑性应变的信息。该方法可以提供一种简单且替代的方式来定性理解微观结构中的取向差和局部塑性应变分布。

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