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反应磁控溅射氧化铝和氮化铝涂层对氧化锆芯体树脂结合强度的影响。

The effect of alumina and aluminium nitride coating by reactive magnetron sputtering on the resin bond strength to zirconia core.

机构信息

Ondokuz Mayis University, Faculty of Dentistry, Department of Prosthodontics, Samsun, Turkey.

Erciyes University, Faculty of Engineering, Department of Mechanical Engineering, Kayseri, Turkey.

出版信息

J Adv Prosthodont. 2013 Nov;5(4):382-7. doi: 10.4047/jap.2013.5.4.382. Epub 2013 Nov 28.

Abstract

PURPOSE

Although several surface treatments have been recently investigated both under in vitro and in vivo conditions, controversy still exists regarding the selection of the most appropriate zirconia surface pre-treatment. The purpose of this study was to evaluate the effect of alumina (Al) and aluminium nitride (AlN) coating on the shear bond strength of adhesive resin cement to zirconia core.

MATERIALS AND METHODS

Fifty zirconia core discs were divided into 5 groups; air particle abrasion with 50 µm aluminum oxide particles (Al2O3), polishing + Al coating, polishing + AlN coating, air particle abrasion with 50 µm Al2O3 + Al coating and air particle abrasion with 50 µm Al2O3 + AlN coating. Composite resin discs were cemented to each of specimens. Shear bond strength (MPa) was measured using a universal testing machine. The effects of the surface preparations on each specimen were examined with scanning electron microscope (SEM). Data were statistically analyzed by one-way ANOVA (α=.05).

RESULTS

The highest bond strengths were obtained by air abrasion with 50 µm Al2O3, the lowest bond strengths were obtained in polishing + Al coating group (P<.05).

CONCLUSION

Al and AlN coatings using the reactive magnetron sputtering technique were found to be ineffective to increase the bond strength of adhesive resin cement to zirconia core.

摘要

目的

尽管最近已经在体外和体内条件下研究了几种表面处理方法,但对于选择最合适的氧化锆表面预处理方法仍存在争议。本研究的目的是评估氧化铝(Al)和氮化铝(AlN)涂层对粘结树脂水门汀与氧化锆基底之间剪切粘结强度的影响。

材料与方法

将 50 个氧化锆基底圆盘分为 5 组;50µm 氧化铝颗粒(Al2O3)空气粒子喷砂、抛光+Al 涂层、抛光+AlN 涂层、50µm Al2O3 空气粒子喷砂+Al 涂层和 50µm Al2O3 空气粒子喷砂+AlN 涂层。将复合树脂圆盘粘结到每个标本上。使用万能试验机测量剪切粘结强度(MPa)。用扫描电子显微镜(SEM)检查每种表面处理方法对各标本的影响。用单因素方差分析(α=.05)对数据进行统计学分析。

结果

用 50µm Al2O3 进行空气喷砂处理的粘结强度最高,抛光+Al 涂层组的粘结强度最低(P<.05)。

结论

使用反应磁控溅射技术的 Al 和 AlN 涂层被发现不能有效提高粘结树脂水门汀与氧化锆基底的粘结强度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/42b9/3865191/c8c91b8feba4/jap-5-382-g001.jpg

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