Kalimuthu Kalpanadevi, Rangasamy Sinduja C, Rakkiyasamy Manimekalai
Acta Chim Slov. 2013;60(4):896-900.
ZnFe₂O₄ nanoparticles have been obtained from the inorganic precursor ZnFe₂(cin)₃(N₂H₄)₃ via thermal decomposition route. The precursor prepared by a simple precipitation method, was characterised by hydrazine and metal analyses, infrared spectral analysis and thermo gravimetric analysis. Using appropriate annealing conditions, ZnFe₂O₄ nanoparticles of average size around 9 nm were synthesised by the thermal treatment of the precursor. The nanoparticles were characterised for their size and structure using X-Ray Diffraction (XRD), High Resolution Transmission Electron Microscopic (HRTEM), Selected Area Electron Diffraction (SAED) and Scanning Electron Microscopic (SEM) techniques.
通过热分解路线，从无机前驱体ZnFe₂(cin)₃(N₂H₄)₃获得了ZnFe₂O₄纳米颗粒。通过简单沉淀法制备的前驱体，通过肼和金属分析、红外光谱分析和热重分析进行了表征。使用适当的退火条件，通过前驱体的热处理合成了平均尺寸约为9 nm的ZnFe₂O₄纳米颗粒。使用X射线衍射（XRD）、高分辨率透射电子显微镜（HRTEM）、选区电子衍射（SAED）和扫描电子显微镜（SEM）技术对纳米颗粒的尺寸和结构进行了表征。
