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利用前散射探测器和电子背散射衍射揭示电工钢的磁畴结构和晶体取向。

Magnetic domain structure and crystallographic orientation of electrical steels revealed by a forescatter detector and electron backscatter diffraction.

机构信息

McGill University, Department of Mining and Materials Engineering, 3610 University Street, Montreal, Quebec, Canada H3A 0C5.

McGill University, Department of Mining and Materials Engineering, 3610 University Street, Montreal, Quebec, Canada H3A 0C5.

出版信息

Ultramicroscopy. 2014 Jul;142:40-9. doi: 10.1016/j.ultramic.2014.03.013. Epub 2014 Apr 13.

Abstract

The magnetic properties of non-oriented electrical steels (NOES) are an important factor in determining the efficiency of electric vehicle drivetrains. Due to the highly variable texture of NOES, the relationships between crystal orientation, the magnetic domain structure, and the final magnetic properties are complicated and not fully understood. In this study, a NOES sample was characterized with a method capable of imaging surface magnetic domains using scanning electron microscopy (SEM) with an electron backscatter diffraction (EBSD) system equipped with a forescatter detector. This method used type II magnetic contrast without a specialized SEM setup, and imaged with a resolution limit of approximately 250-300nm. The domain structure of the NOES sample was successfully related to β, which was defined as the angle between the closest magnetic easy axis and the surface of the sample (the RD-TD plane). However, it was shown that if the easy axes were aligned between neighbouring grains with respect to the grain boundary normal, the domain structure could align with an easy axis that was not the closest to the surface, and complex domain structures could be become wider. This structure and width change of complex domain structures has not been previously observed from single crystal or large-grained material studies. The successful application of this method to reveal the influence of surrounding grains can be used to better understand the magnetic properties of NOES.

摘要

非取向电工钢(NOES)的磁性能是决定电动汽车传动系统效率的一个重要因素。由于 NOES 的织构高度各向异性,因此晶体取向、磁畴结构与最终磁性能之间的关系非常复杂,目前尚未完全清楚。在这项研究中,我们使用配备前散射探测器的电子背散射衍射(EBSD)系统的扫描电子显微镜(SEM)对 NOES 样品进行了表面磁畴成像的特性分析。该方法使用了 II 型磁对比,无需专门的 SEM 设备,分辨率约为 250-300nm。NOES 样品的畴结构与β成功相关联,β定义为最接近磁易轴与样品表面(RD-TD 平面)之间的夹角。然而,研究表明,如果易轴相对于晶界法线在相邻晶粒之间对齐,则畴结构可能与最接近表面的易轴不一致,并且复杂的畴结构可能变宽。这种畴结构的变化和复杂畴结构的宽度变化以前从未在单晶或大晶粒材料研究中观察到过。该方法成功地应用于揭示周围晶粒的影响,可以用来更好地理解 NOES 的磁性能。

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