Department of Prosthodontics, Veterans Health Service Medical Center, 6-2, Doonchon-dong, Kangdong-gu, Seoul, Republic of Korea; Department of Prosthodontics and Dental Research Institute, School of Dentistry, Seoul National University, 275-1, Yeongeon-dong, Jongno-gu, Seoul, Republic of Korea.
Department of Prosthodontics and Dental Research Institute, School of Dentistry, Seoul National University, 275-1, Yeongeon-dong, Jongno-gu, Seoul, Republic of Korea.
Dent Mater. 2014 Sep;30(9):e229-37. doi: 10.1016/j.dental.2014.04.008. Epub 2014 May 20.
This study was aimed to investigate the effect of the number of coloring liquid applications on the optical properties of monolithic zirconia.
Eighteen monolithic zirconia specimens (27.6 mm×27.6 mm×2.0 mm) were fabricated and divided into 6 groups (n=3). Each group was designated by the number of A2-coloring liquid applications (Group I to Group V) and Group O as a control. Color and spectral distribution of the specimens were measured with a double-beam spectrophotometer. CIE L*, a* and b* relative to the standard illuminants D65 were measured in reflectance and transmittance modes. Color difference (ΔEab*), translucency parameter (TP) and opalescence parameter (OP) were calculated. All measurements were performed on five different areas of each specimen. All data were analyzed by ANOVA and multiple comparison Scheffé test, Pearson correlations and linear regression analysis (α=0.05).
With the increase of the number of coloring liquid applications, CIE L* (R2=0.878) and OP values (R2=0.701) were decreased, but CIE b* (R2=0.938) was increased. However, TP values were not significantly changed. The color differences among groups ranged from 1.3 to 15.7 ΔEab* units. Strong correlation was found between OP and Δb* (R2=0.982, P<.01).
Within the limitations of this study, it can be concluded that the number of coloring liquid applications with a single shade affects the lightness, yellow chromaticity and opalescence of monolithic zirconia, although its translucency cannot be controlled by the coloring procedure.
本研究旨在探讨上釉次数对整体氧化锆光学性能的影响。
制备 18 个 27.6mm×27.6mm×2.0mm 的整体氧化锆试件,分为 6 组(n=3)。每组根据 A2 色料上釉次数(I 组至 V 组)和对照组(O 组)进行分组。采用分光光度计测量试件的颜色和光谱分布。分别在反射和透射模式下测量试样相对于标准光源 D65 的 CIE L*、a和 b值。计算颜色差异(ΔEab*)、半透明度参数(TP)和乳光参数(OP)。在每个试件的五个不同区域进行所有测量。采用方差分析和多重比较 Scheffé 检验、Pearson 相关和线性回归分析(α=0.05)对所有数据进行分析。
随着上釉次数的增加,CIE L*(R2=0.878)和 OP 值(R2=0.701)降低,而 CIE b*(R2=0.938)升高。然而,TP 值没有显著变化。组间颜色差异在 1.3 到 15.7 ΔEab单位之间。OP 与 Δb之间存在强相关性(R2=0.982,P<.01)。
在本研究的限制范围内,可以得出结论,单一色调的上釉次数会影响整体氧化锆的明度、黄度和乳光度,但其半透明度不能通过上釉程序控制。