Bagheri R, Fani M, Barfi Ghasrodashti Ar, Nouri Yadkouri N, Mousavi Sm
Dept. of Dental Materials and Biomaterial Research Centre, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
Student Research Committee, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.
J Dent (Shiraz). 2014 Jun;15(2):74-80.
Resin composites are brittle materials and their major shortcomings are manifested in their sensitivity to flaws and defects. Although various mechanical properties of resin composites have been described, few studies are available on assessing the effect of bleaching agents on resin composites using the short rod design.
To place various resin composites into distilled water at 37°C for 21 days and determine the effect of immersion time in distilled water, with and without exposure to 10% carbamide peroxide by employing short rod design fracture toughness test.
Specimens were prepared from three resin composites; Rok (SDI), Esthet (Dentsply), and Estelite (Tokuyama). For each material, a total of 24 disc-shaped specimens were prepared using a custom-made mould. Specimens were randomly divided into 3 groups of 8 and conditioned in 37°C distilled water for either 24 hours, or 21 days. 21 day specimens were tested both with and without applying bleaching agent; Polanight (SDI). Study group specimens were bleached for 21 days, 2 hours a day. The specimens were loaded using a universal testing machine with a crosshead speed of 0.5 mm per minute. The maximum load at specimen failure was recorded and the KIc (MPa. M (0.5)) was calculated.
Statistical analysis using two-way ANOVA showed a significant relationship between material and time (p< 0.05).Tukey's test showed that after 24 h of immersion in distilled water, Rok revealed the highest KIc followed by Esthet and Estelite. The bleaching agent significantly improved the fracture toughness values of Esthet while it decreased that of Estelite.
The fracture toughness of the resin composites was affected by the bleaching agent and distilled water. In comparison with Rok and Estelite, fracture toughness of Esthet was increased due to aging and application of bleaching agent.
树脂复合材料是脆性材料,其主要缺点表现为对裂纹和缺陷敏感。尽管已经描述了树脂复合材料的各种力学性能,但很少有研究采用短棒设计来评估漂白剂对树脂复合材料的影响。
将各种树脂复合材料在37°C的蒸馏水中放置21天,通过采用短棒设计断裂韧性试验,确定在有和没有暴露于10%过氧化脲的情况下,浸泡时间在蒸馏水中的影响。
从三种树脂复合材料制备试样;Rok(SDI)、Esthet(登士柏)和Estelite(德山)。对于每种材料,使用定制模具制备总共24个圆盘形试样。试样随机分为3组,每组8个,并在37°C蒸馏水中分别处理24小时或21天。对21天的试样在使用和不使用漂白剂Polanight(SDI)的情况下进行测试。研究组试样每天漂白2小时,共漂白21天。使用万能试验机以每分钟0.5毫米的十字头速度加载试样。记录试样破坏时的最大载荷,并计算KIc(MPa·M(0.5))。
使用双向方差分析的统计分析表明材料和时间之间存在显著关系(p<0.05)。Tukey检验表明,在蒸馏水中浸泡24小时后,Rok的KIc最高,其次是Esthet和Estelite。漂白剂显著提高了Esthet的断裂韧性值,而降低了Estelite的断裂韧性值。
树脂复合材料的断裂韧性受漂白剂和蒸馏水的影响。与Rok和Estelite相比,Esthet的断裂韧性由于老化和漂白剂的应用而增加。