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抗冲刷型三氧化矿物凝聚体的压汞孔隙率测定及水泥-牙本质界面评估

Mercury intrusion porosimetry and assessment of cement-dentin interface of anti-washout-type mineral trioxide aggregate.

作者信息

Formosa L M, Damidot D, Camilleri Josette

机构信息

Department of Metallurgy and Materials Engineering, Faculty of Engineering, University of Malta, Malta.

University of Lille Nord de France, Lille, France; EM Douai, Douai, France.

出版信息

J Endod. 2014 Jul;40(7):958-63. doi: 10.1016/j.joen.2013.11.015. Epub 2014 Jan 3.

DOI:10.1016/j.joen.2013.11.015
PMID:24935543
Abstract

INTRODUCTION

One of the disadvantages of mineral trioxide aggregate (MTA) is washout (ie, the tendency of freshly prepared cement paste to disintegrate upon early contact with physiological fluids). A novel MTA (MTA Plus; Prevest Denpro, Jammu City, India) exhibits low washout and superior physical properties when mixed with a gel instead of water. When used as a root-end filler, MTA is in contact with both bone and root dentin. This study aimed to investigate the porosity and interfacial characteristics of the novel MTA mixed with water or antiwashout gel.

METHODS

Porosity was evaluated after 1 or 28 days of immersion in Hank's balanced salt solution using mercury intrusion porosimetry. The root dentin to material interface was investigated using a scanning electron microscope and energy-dispersive X-ray spectroscopy complete with line scans and elemental maps.

RESULTS

Anti-washout-type MTA Plus was found to have lower initial porosity than MTA Plus mixed with water although this trend was reversed after 28 days of immersion in physiological fluid. Both materials exhibited good marginal adaptation. The diffusion of silicon, calcium, and phosphorus across the cement/dentin interface was observed.

CONCLUSIONS

MTA Plus mixed with antiwashout gel was found to have lower initial porosity than MTA Plus mixed with water. Both materials exhibited good marginal adaptation and the diffusion of silicon, calcium, and phosphorous across the cement/dentin interface. Thus, the anti-washout-type MTA can be considered to be a suitable substitute for ordinary MTA in all its indications.

摘要

引言

三氧化矿物凝聚体(MTA)的缺点之一是易被冲洗掉(即新制备的水泥浆在早期与生理流体接触时会解体的趋势)。一种新型MTA(MTA Plus;印度查谟市Prevest Denpro公司)与凝胶而非水混合时,冲洗流失率低且物理性能优越。当用作根尖充填材料时,MTA会与骨组织和牙根牙本质接触。本研究旨在探究新型MTA与水或抗冲洗凝胶混合后的孔隙率和界面特征。

方法

使用压汞法在汉克平衡盐溶液中浸泡1天或28天后评估孔隙率。使用扫描电子显微镜和能量色散X射线光谱仪并结合线扫描和元素图谱研究牙根牙本质与材料的界面。

结果

发现抗冲洗型MTA Plus的初始孔隙率低于与水混合的MTA Plus,尽管在生理流体中浸泡28天后这种趋势发生了逆转。两种材料均表现出良好的边缘适应性。观察到硅、钙和磷在水门汀/牙本质界面的扩散。

结论

发现与抗冲洗凝胶混合的MTA Plus的初始孔隙率低于与水混合的MTA Plus。两种材料均表现出良好的边缘适应性以及硅、钙和磷在水门汀/牙本质界面的扩散。因此,抗冲洗型MTA可被认为是普通MTA在所有适应证中的合适替代品。

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