• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

3-甲基硫烷基-5-苯基-1,2,4-三嗪

3-Methyl-sulfanyl-5-phenyl-1,2,4-triazine.

作者信息

Hamri Salha, Hafid Abderrafia, Khouili Mostafa, El Ammari Lahcen, Ketatni El Mostafa

机构信息

Laboratoire de Chimie Organique et Analytique, Université Sultan Moulay Slimane, Faculté des Sciences et Techniques, BP 523, 23000 Béni-Mellal, Morocco.

Laboratoire de Chimie du Solide Appliquée, Faculté des Sciences, Université Mohammed V-Agdal, Avenue Ibn Battouta, BP 1014, Rabat, Morocco.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2014 May 31;70(Pt 6):o720. doi: 10.1107/S1600536814011830. eCollection 2014 Jun 1.

DOI:10.1107/S1600536814011830
PMID:24940289
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4051076/
Abstract

In the mol-ecule of the title compound, C10H9N3S, the dihedral angle between the triazine and phenyl rings is 11.77 (7)°. In the crystal, mol-ecules are linked by π-π stacking inter-actions [centroid-centroid distances = 3.7359 (3) and 3.7944 (4) Å], forming layers parallel to the bc plane.

摘要

在标题化合物C₁₀H₉N₃S的分子中，三嗪环和苯环之间的二面角为11.77 (7)°。在晶体中，分子通过π-π堆积相互作用相连[质心-质心距离 = 3.7359 (3) 和3.7944 (4) Å]，形成平行于bc平面的层。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e78c/4051076/6f9c101e0a8e/e-70-0o720-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e78c/4051076/6f9c101e0a8e/e-70-0o720-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e78c/4051076/6f9c101e0a8e/e-70-0o720-fig1.jpg

相似文献

1
3-Methyl-sulfanyl-5-phenyl-1,2,4-triazine.3-甲基硫烷基-5-苯基-1,2,4-三嗪
Acta Crystallogr Sect E Struct Rep Online. 2014 May 31;70(Pt 6):o720. doi: 10.1107/S1600536814011830. eCollection 2014 Jun 1.
2
5-(4-Bromo-phen-yl)-2-(3,4-methyl-ene-dioxy-phen-yl)-3-methyl-sulfanyl-1-benzofuran.5-（4-溴苯基）-2-（3,4-亚甲二氧基苯基）-3-甲基硫烷基-1-苯并呋喃
Acta Crystallogr Sect E Struct Rep Online. 2009 Sep 26;65(Pt 10):o2530. doi: 10.1107/S1600536809038148.
3
2-Eth-oxy-4-(4-methyl-phen-yl)-6-phenyl-pyridine-3-carbonitrile.2-乙氧基-4-（4-甲基苯基）-6-苯基吡啶-3-腈
Acta Crystallogr Sect E Struct Rep Online. 2012 Aug 1;68(Pt 8):o2495-6. doi: 10.1107/S1600536812032163. Epub 2012 Jul 18.
4
5-Chloro-2-methyl-3-phenyl-sulfonyl-1-benzofuran.5-氯-2-甲基-3-苯基磺酰基-1-苯并呋喃
Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 7;64(Pt 7):o1190. doi: 10.1107/S1600536808015699.
5
1-Methyl-2-methyl-sulfanyl-6-nitro-1H-benzimidazole.1-甲基-2-甲硫基-6-硝基-1H-苯并咪唑
Acta Crystallogr Sect E Struct Rep Online. 2014 Mar 8;70(Pt 4):o407. doi: 10.1107/S1600536814004723. eCollection 2014 Apr 1.
6
Crystal structure of phenyl -(3,5-di-methyl-phenyl)carbamate.苯基-（3,5-二甲基苯基）氨基甲酸酯的晶体结构
Acta Crystallogr E Crystallogr Commun. 2017 May 12;73(Pt 6):849-852. doi: 10.1107/S2056989017006922. eCollection 2017 Jun 1.
7
1,1'-{2,2'-[1,4-Phenyl-enebis(methyl-ene)]bis-(-oxy)bis-(2,1-phenyl-ene)}diethanone.1,1'-{2,2'-[1,4-亚苯基双(亚甲基)]双(-氧基)双-(2,1-亚苯基)}二乙酮
Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):o3016. doi: 10.1107/S1600536811042528. Epub 2011 Oct 22.
8
5-Isopropyl-2-methyl-3-phenyl-sulfonyl-1-benzofuran.5-异丙基-2-甲基-3-苯基磺酰基-1-苯并呋喃
Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 13;64(Pt 7):o1257. doi: 10.1107/S1600536808017224.
9
(E)-4-(2-Hy-droxy-3-meth-oxy-benzyl-idene-amino)-6-methyl-3-sulfanyl-idene-3,4-dihydro-1,2,4-triazin-5(2H)-one.（E）-4-（2-羟基-3-甲氧基-亚苄基氨基）-6-甲基-3-硫亚基-3,4-二氢-1,2,4-三嗪-5（2H）-酮
Acta Crystallogr Sect E Struct Rep Online. 2012 Sep 1;68(Pt 9):o2815. doi: 10.1107/S1600536812036756. Epub 2012 Aug 31.
10
Crystal structure of 4-methyl-sulfanyl-2-phenyl-quinazoline.4-甲基硫烷基-2-苯基喹唑啉的晶体结构
Acta Crystallogr Sect E Struct Rep Online. 2014 Jul 23;70(Pt 8):o919-20. doi: 10.1107/S1600536814015657. eCollection 2014 Aug 1.

本文引用的文献

1
Structure validation in chemical crystallography.化学晶体学中的结构验证
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
3
Antinociceptive activity of new imidazolidine carbonyl derivatives. Part 4. Synthesis and pharmacological activity of 8-aryl-3,4-dioxo-2H,8H-6,7-dihydroimidazo[2,1-c] [1,2,4]triazines.
新型咪唑烷羰基衍生物的抗伤害感受活性。第4部分。8-芳基-3,4-二氧代-2H,8H-6,7-二氢咪唑并[2,1-c][1,2,4]三嗪的合成与药理活性。
Eur J Med Chem. 2005 Feb;40(2):127-34. doi: 10.1016/j.ejmech.2004.09.020.
4
DNA-targeted 1,2,4-benzotriazine 1,4-dioxides: potent analogues of the hypoxia-selective cytotoxin tirapazamine.靶向DNA的1,2,4-苯并三嗪-1,4-二氧化物：低氧选择性细胞毒素替拉扎明的强效类似物。
J Med Chem. 2004 Jan 15;47(2):475-88. doi: 10.1021/jm030399c.
5
Synthesis of some new biologically active bis-(thiadiazolotriazines) and bis-(thiadiazolotriazinyl) alkanes.一些新型生物活性双（噻二唑并三嗪）和双（噻二唑并三嗪基）烷烃的合成
Farmaco. 2001 Dec;56(12):899-903.
6
Synthesis of heterobicyclic nitrogen systems bearing the 1,2,4-triazine moiety as anti-HIV and anticancer drugs: Part I.含1,2,4-三嗪部分的杂双环氮系统作为抗HIV和抗癌药物的合成：第一部分。
Pharmazie. 1999 May;54(5):347-51.
7
Synthesis and anti-inflammatory activity of some novel 1,3,4-oxadiazole derivatives.一些新型1,3,4-恶二唑衍生物的合成及其抗炎活性
J Chem Technol Biotechnol. 1992;53(2):143-6. doi: 10.1002/jctb.280530206.