Anderson Brian J, Shalit Zachary A, Jasinski Jerry P
Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USA.
Acta Crystallogr Sect E Struct Rep Online. 2014 May 31;70(Pt 6):o732. doi: 10.1107/S1600536814012057. eCollection 2014 Jun 1.
In the title compound, C15H17N3OS, the dihedral angle between the mean planes of the 2-hy-droxy-napthyl ring system and the hydrazinecarbo-thio-amide group is 73.7 (3)°. In the crystal, weak O-H⋯S and C-H⋯O inter-actions and π-π stacking inter-actions involving one of the hy-droxy-napthyl rings with a centroid-centroid distance of 3.6648 (14) Å are observed, forming infinite chains along [010]. In addition, N-H⋯S inter-actions occur.
在标题化合物C₁₅H₁₇N₃OS中,2-羟基萘环体系的平均平面与肼基碳硫酰胺基团之间的二面角为73.7 (3)°。在晶体中,观察到弱的O-H⋯S和C-H⋯O相互作用以及涉及其中一个羟基萘环的π-π堆积相互作用,其质心间距为3.6648 (14) Å,沿[010]方向形成无限链。此外,还存在N-H⋯S相互作用。