2-[1-(2-羟基-6-甲氧基苯基)亚乙基]-N-甲基肼基甲硫酰胺乙腈单溶剂合物
2-[1-(2-Hy-droxy-6-meth-oxy-phen-yl)ethyl-idene]-N-methyl-hydrazinecarbothio-amide acetonitrile monosolvate.
作者信息
Anderson Brian J, Keeler Alexander M, O'Rourke Kelly A, Krauss Shannon T, Jasinski Jerry P
机构信息
Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USA.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2013 Jan 1;69(Pt 1):o11. doi: 10.1107/S1600536812048799. Epub 2012 Dec 5.
Abstract
In the title compound, C11H15N3O2S·C2H3N, the dihedral angle between the benzene ring and the mean plane of the hydrazinecarbothio-amide group is 75.1 (2)°. In the crystal, the main mol-ecule is linked to the solvent mol-ecule by a weak N-H⋯N hydrogen bond while O-H⋯S hydrogen bonds link the mol-ecules into columns along [100].
摘要
在标题化合物C₁₁H₁₅N₃O₂S·C₂H₃N中，苯环与肼基碳硫酰胺基团平均平面之间的二面角为75.1 (2)°。在晶体中，主要分子通过弱的N-H⋯N氢键与溶剂分子相连，而O-H⋯S氢键将分子沿[100]方向连接成列。
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