Spyrou Maria, Koliniotou-Koumpia Eugenia, Kouros Pantelis, Koulaouzidou Elisabeth, Dionysopoulos Pavlos
Department of Operative Dentistry, Dental School of Aristotle University of Thessaloniki, Thessaloniki, Greece.
Eur J Dent. 2014 Jul;8(3):353-359. doi: 10.4103/1305-7456.137647.
The objective was to investigate the way that various surface treatments could influence the bond strength of the repair of methacrylate (MC) and silorane (SIL) composites.
A total of 160 MC and SIL cylindrical specimens were polymerized and aged in artificial saliva solution for 7 days. Depending on the following surface treatment (diamond bur or air abrasion), and the conditioning procedure (orthophosphoric acid or sodium hypochlorite), 16 groups were formed and repaired either with MC, either with SIL composite. Repaired specimens were subjected to an additional aging procedure in artificial saliva for 7 days, followed by thermo-cycling and then stressed in shear at a rate of 0.5 mm/min until failure. Failure patterns were analyzed using stereomicroscope and scanning electron microscopy.
MC composite showed statistically significant higher bond strength both as a base or repair material than SIL (P < 0.001). Statistically significant differences were not observed, when grinding and conditioning procedures was compared. Pretest failures were observed when aged MC-based composite was repaired with SIL-based.
Type of composite seems to be the main factor influencing the bond strength of the repair. MC-based composite showed better repairability than SIL composite. Optimum repair conditions should include knowledge of the composite's composition.
研究各种表面处理方式对甲基丙烯酸酯(MC)和硅烷(SIL)复合材料修复粘结强度的影响。
共制备160个MC和SIL圆柱形试件,在人工唾液溶液中聚合并老化7天。根据以下表面处理(金刚砂车针或空气喷砂)和预处理程序(正磷酸或次氯酸钠),形成16组,分别用MC或SIL复合材料进行修复。修复后的试件在人工唾液中再进行7天的老化处理,然后进行热循环,接着以0.5 mm/min的速率进行剪切应力测试直至破坏。使用体视显微镜和扫描电子显微镜分析破坏模式。
MC复合材料作为基底材料或修复材料时,其粘结强度在统计学上均显著高于SIL(P < 0.001)。比较研磨和预处理程序时,未观察到统计学上的显著差异。当用基于SIL的材料修复老化的基于MC的复合材料时,观察到预测试失败。
复合材料类型似乎是影响修复粘结强度的主要因素。基于MC的复合材料比SIL复合材料具有更好的可修复性。最佳修复条件应包括对复合材料成分的了解。